枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数500
标示量(mg)25供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.362380762380192384902383752381112382140.09
217.312380292377502378900.09
单位质量响应值RSD%判断
13722.0013742.920.11数据可信
供试品溶液-2024051611批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1269419-26941999.34198.371.5299.3498.371.52
2260222-26022295.95095.95
3265074-26507497.73997.74
4265834-26583498.01998.02
5268385-26838598.95998.96
6271782-271782100.212100.21
10min1272705-272705100.552100.212.32100.72100.382.32
2263329-26332997.09597.26
3268080-26808098.84799.01
4269720-26972099.45299.62
5281543-281543103.811103.98
6275344-275344101.525101.69
15min1272128-272128100.34099.511.45100.6799.841.44
2263792-26379297.26697.59
3268031-26803198.82999.16
4269185-26918599.25499.58
5270841-27084199.865100.20
6275240-275240101.487101.82
20min1271980-271980100.28599.331.57100.7999.821.57
2262679-26267996.85697.34
3268136-26813698.86899.36
4268272-26827298.91899.41
5270069-27006999.580100.08
6275174-275174101.463101.97
30min1270968-27096899.91298.931.37100.5899.591.37
2262088-26208896.63897.28
3266957-26695798.43399.09
4267880-26788098.77399.43
5269446-26944699.351100.02
6272504-272504100.478101.15
45min1270292-27029299.66399.370.85100.50100.200.85
2269632-26963299.419100.23
3266829-26682998.38699.21
4267799-26779998.74399.57
5269059-26905999.208100.04
6273394-273394100.806101.65
极限1270325-27032599.67598.901.34100.6799.891.34
2263051-26305196.99397.96
3266309-26630998.19499.18
4267601-26760198.67099.66
5268379-26837998.95799.96
6273632-273632100.894101.90
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