枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数500
标示量(mg)25供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.362381162370942382552377572377902378020.19
217.312371692372682372180.03
单位质量响应值RSD%判断
13698.2713704.100.04数据可信
供试品溶液-2024051611批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1272251-272251100.61498.002.01100.6198.002.01
2268694-26869499.30099.30
3262823-26282397.13097.13
4265979-26597998.29698.30
5264748-26474897.84197.84
6256634-25663494.84394.84
10min1276514-276514102.19099.352.09102.3699.522.09
2270854-270854100.098100.26
3264532-26453297.76197.92
4271146-271146100.206100.37
5269474-26947499.58899.75
6260498-26049896.27196.43
15min1276119-276119102.04499.272.31102.3899.602.31
2271415-271415100.305100.64
3263699-26369997.45497.78
4270537-27053799.981100.31
5271044-271044100.168100.50
6258906-25890695.68296.00
20min1274139-274139101.31298.892.03101.8299.382.03
2270598-270598100.003100.50
3263809-26380997.49497.98
4268660-26866099.28799.78
5269499-26949999.597100.09
6258850-25885095.66296.14
30min1272683-272683100.77498.601.94101.4599.261.94
2268746-26874699.31999.98
3263381-26338197.33697.99
4269637-26963799.648100.31
5268120-26812099.08799.75
6258225-25822595.43196.07
45min1273672-273672101.13999.331.31101.98100.151.31
2269043-26904399.429100.26
3262704-26270497.08697.90
4269546-26954699.614100.44
5268768-26876899.327100.15
6268878-26887899.368100.16
极限1273321-273321101.01098.362.44102.0299.352.43
2269101-26910199.450100.45
3260526-26052696.28197.25
4270112-27011299.824100.82
5267740-26774098.94799.94
6256148-25614894.66395.63
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