枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数500
标示量(mg)25供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.362397292399332401822399222400702399670.08
217.312396262395582395920.03
单位质量响应值RSD%判断
13822.9813841.250.10数据可信
供试品溶液-2024051611批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1263338-26333896.39996.471.0996.4096.481.09
2264309-26430996.75496.75
3261148-26114895.59795.60
4263291-26329196.38296.38
5268603-26860398.32698.33
6260584-26058495.39195.39
10min1265674-26567497.25497.221.3897.4197.381.38
2264829-26482996.94597.11
3261735-26173595.81295.97
4270484-27048499.01599.18
5269131-26913198.52098.68
6261693-26169395.79795.96
15min1274655-274655100.54297.512.35100.8697.832.34
2263471-26347196.44896.77
3260005-26000595.17995.50
4272441-27244199.731100.06
5267474-26747497.91398.24
6260123-26012395.22295.54
20min1261908-26190895.87696.351.8096.3796.841.80
2262150-26215095.96496.45
3259164-25916494.87195.35
4271416-27141699.35699.85
5265758-26575897.28597.78
6258880-25888094.76795.24
30min1261703-26170395.80095.851.5496.4596.501.54
2260805-26080595.47296.12
3257883-25788394.40295.04
4268142-26814298.15898.82
5264717-26471796.90497.56
6257844-25784494.38895.02
45min1259660-25966095.05395.311.7195.8696.111.71
2259483-25948394.98895.79
3257016-25701694.08594.88
4267957-26795798.09098.91
5262567-26256796.11796.93
6255453-25545393.51394.31
极限1258452-25845294.61095.892.5295.5896.862.49
2257093-25709394.11395.07
3271823-27182399.505100.45
4267225-26722597.82298.81
5262600-26260096.12997.10
6254538-25453893.17894.13
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