枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数500
标示量(mg)25供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.364732734737134741564743754741064739250.10
217.314723474727054725260.06
单位质量响应值RSD%判断
27299.8327297.860.01数据可信
供试品溶液-2024051711批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1523426-52342697.08696.980.1997.0996.980.19
2522146-52214696.84996.85
3521554-52155496.73996.74
4522851-52285196.98096.98
5524319-52431997.25297.25
6522931-52293196.99596.99
10min1532787-53278798.82398.810.1998.9898.980.19
2531960-53196098.66998.83
3531622-53162298.60798.77
4532337-53233798.73998.90
5534251-53425199.09499.26
6533471-53347198.95099.11
15min1529278-52927898.17298.410.3998.5098.740.39
2533202-53320298.90099.23
3528606-52860698.04798.37
4528537-52853798.03498.36
5531318-53131898.55098.88
6532531-53253198.77599.10
20min1525660-52566097.50197.860.2597.9998.350.25
2529661-52966198.24398.73
3527161-52716197.77998.27
4527756-52775697.89098.38
5528039-52803997.94298.43
6527429-52742997.82998.32
30min1528924-52892498.10697.560.4098.7698.220.40
2526487-52648797.65498.31
3525509-52550997.47398.12
4523313-52331397.06597.72
5524236-52423697.23797.89
6527551-52755197.85298.51
45min1526155-52615597.59397.150.4098.4197.960.40
2525775-52577597.52298.34
3521608-52160896.74997.56
4521076-52107696.65197.47
5524240-52424097.23798.05
6523650-52365097.12897.95
极限1524433-52443397.27396.760.4998.2597.740.48
2525128-52512897.40298.38
3520727-52072796.58697.56
4518760-51876096.22197.20
5520694-52069496.58097.56
6520193-52019396.48797.47
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