枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数500
标示量(mg)25供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.369552779560599589719556439567169565330.16
217.319548649561319554980.10
单位质量响应值RSD%判断
55099.8355199.190.13数据可信
供试品溶液-2024051911批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11033444-103344494.88493.841.0594.8893.841.05
21016075-101607593.28993.29
31014325-101432593.12993.13
41013246-101324693.03093.03
51017383-101738393.40993.41
61037818-103781895.28695.29
10min11065154-106515497.79597.200.6997.9597.360.69
21057233-105723397.06897.22
31053096-105309696.68896.84
41048458-104845896.26396.42
51060691-106069197.38697.54
61067603-106760398.02098.18
15min11072220-107222098.44497.990.6398.7798.310.63
21066955-106695597.96198.28
31059343-105934397.26297.58
41061567-106156797.46697.78
51066046-106604697.87798.20
61077237-107723798.90599.23
20min11075506-107550698.74698.020.5799.2398.500.57
21067840-106784098.04298.52
31061290-106129097.44197.92
41061065-106106597.42097.90
51066417-106641797.91198.39
61073640-107364098.57599.06
30min11073109-107310998.52697.910.4999.1898.550.50
21065157-106515797.79698.44
31062383-106238397.54198.18
41061209-106120997.43398.07
51063690-106369097.66198.31
61072635-107263598.48299.13
45min11068269-106826998.08197.620.5798.9098.430.58
21059218-105921897.25098.06
31057886-105788697.12897.93
41060151-106015197.33698.14
51061020-106102097.41698.22
61073176-107317698.53299.35
极限11062217-106221797.52697.010.4998.5097.980.49
21055127-105512796.87597.84
31052531-105253196.63697.60
41051582-105158296.54997.51
51054277-105427796.79797.77
61063839-106383997.67598.65
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