坎地沙坦酯左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100685-201903对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数1000
标示量(mg)8供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.087559575754756707566475670756710.08
216.137631276396763540.08
单位质量响应值RSD%判断
4705.914733.660.42数据可信
供试品溶液-24020104批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min111989-1198957.04051.835.8557.0451.835.85
210847-1084751.60651.61
310746-1074651.12651.13
410845-1084551.59751.60
510000-1000047.57747.58
610936-1093652.03052.03
10min122980-22980109.331107.033.80109.97107.603.81
222817-22817108.556109.13
322597-22597107.509108.08
422727-22727108.128108.70
520786-2078698.89399.42
623065-23065109.736110.31
15min131573-31573150.214146.662.25152.06148.422.27
230832-30832146.689148.47
330710-30710146.108147.87
431502-31502149.876151.65
529664-29664141.132142.76
630674-30674145.937147.73
20min137119-37119176.600176.492.77180.12179.882.76
237634-37634179.050182.46
336172-36172172.095175.48
437839-37839180.026183.47
535585-35585169.302172.50
638220-38220181.838185.26
30min146046-46046219.072218.482.28224.55223.842.28
245128-45128214.704220.10
345839-45839218.087223.39
447195-47195224.538229.98
544422-44422211.345216.42
646899-46899223.130228.57
45min154146-54146257.609256.591.50265.52264.371.50
253413-53413254.122261.91
353544-53544254.745262.47
453753-53753255.739263.67
553272-53272253.451260.88
655461-55461263.865271.78
60min159281-59281282.040283.451.32292.82294.091.29
259236-59236281.825292.43
358418-58418277.934288.49
460705-60705288.814299.59
559860-59860284.794295.04
659967-59967285.303296.15
极限165066-65066309.563311.961.35323.47325.741.24
265798-65798313.045326.78
365071-65071309.586323.23
464911-64911308.825322.81
567255-67255319.977333.38
665319-65319310.766324.79
坎地沙坦酯左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100685-201903对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数1000
标示量(mg)8供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.087608576053760407599776011760370.05
216.137778077967778740.17
单位质量响应值RSD%判断
4728.674827.901.47数据可信
供试品溶液-24020103批-pH1.2(内含0.05%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min146536-46536218.714207.184.48218.71207.184.48
244414-44414208.741208.74
343319-43319203.595203.59
441932-41932197.076197.08
542127-42127197.992197.99
646160-46160216.947216.95
10min166612-66612313.069304.101.99315.50306.402.00
264246-64246301.949304.27
364917-64917305.103307.37
462907-62907295.656297.85
564030-64030300.934303.13
665507-65507307.876310.29
15min172919-72919342.711337.862.39348.62343.542.39
271414-71414335.638341.31
370670-70670332.141337.79
469981-69981328.903334.38
571583-71583336.432341.98
674756-74756351.345357.18
20min174841-74841351.745349.961.55361.46359.401.55
273376-73376344.859354.26
374467-74467349.987359.33
472849-72849342.382351.51
575497-75497354.828364.11
675744-75744355.989365.72
30min176636-76636360.181362.081.44373.81375.401.42
275930-75930356.863370.10
376274-76274358.480371.71
476533-76533359.697372.63
578475-78475368.824382.05
678390-78390368.425382.12
45min174513-74513350.203354.311.60367.83371.661.48
276345-76345358.813376.01
373857-73857347.120364.33
476784-76784360.877377.81
576212-76212358.188375.51
674609-74609350.654368.44
60min176622-76622360.115359.200.70381.63380.480.68
276071-76071357.526378.71
377307-77307363.335384.41
475742-75742355.979376.92
576406-76406359.100380.40
676416-76416359.147380.83
极限174794-74794351.524350.120.78377.04375.400.80
273768-73768346.702371.86
374340-74340349.390374.50
473965-73965347.628372.52
574804-74804351.571376.86
675304-75304353.921379.59
坎地沙坦酯左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100685-201903对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数1000
标示量(mg)8供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.087768077632776777775877681776860.06
216.137742777408774180.02
单位质量响应值RSD%判断
4831.224799.630.47数据可信
供试品溶液-24020104批-pH1.2(内含0.05%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min132964-32964153.717150.573.13153.72150.573.13
231286-31286145.893145.89
333763-33763157.443157.44
431129-31129145.160145.16
532076-32076149.577149.58
632515-32515151.624151.62
10min153666-53666250.255243.672.31251.96245.342.31
252206-52206243.447245.07
352683-52683245.671247.42
450284-50284234.484236.10
553110-53110247.662249.32
651569-51569240.476242.16
15min159943-59943279.526277.871.62284.01282.251.62
259995-59995279.768284.09
359830-59830278.999283.48
457639-57639268.782273.00
559936-59936279.493283.91
660187-60187280.664285.02
20min161431-61431286.465293.711.36294.06301.181.32
263551-63551296.350303.79
363607-63607296.612304.19
462610-62610291.962299.17
563121-63121294.345301.86
663588-63588296.523304.00
30min166156-66156308.498311.462.26319.28322.202.22
266594-66594310.541321.27
366786-66786311.436322.31
464409-64409300.351310.80
568337-68337318.669329.46
668468-68468319.279330.05
45min167960-67960316.910318.511.66331.12332.701.65
268251-68251318.267332.45
369405-69405323.649337.98
466499-66499310.098323.88
569626-69626324.679339.01
668081-68081317.475331.79
60min168461-68461319.247319.811.71336.97337.541.69
269367-69367323.472341.19
369103-69103322.241340.17
466289-66289309.118326.35
569030-69030321.900339.84
669242-69242322.889340.73
极限170774-70774330.033328.301.29351.31349.581.27
269582-69582324.474345.78
369982-69982326.339347.85
469375-69375323.509344.18
571698-71698334.342355.86
671001-71001331.091352.52
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