比索洛尔氨氯地平片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)0
对照品批号100711-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.608695786546867638697687023868530.23
210.528699186951869710.04
单位质量响应值RSD%判断
8193.688267.210.64数据可信
供试品溶液-2024021621批-比索洛尔-0.005hcl
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min190185-9018598.42298.261.6198.4298.261.61
288212-8821296.26996.27
391472-9147299.82799.83
488331-8833196.39996.40
591359-9135999.70399.70
690656-9065698.93698.94
10min190579-9057998.85298.991.9999.0299.161.99
288874-8887496.99197.15
391899-91899100.293100.46
488490-8849096.57296.73
593193-93193101.705101.87
691202-9120299.53299.70
15min190278-9027898.52498.651.9698.8598.981.96
288718-8871896.82197.14
391680-91680100.054100.39
488251-8825196.31296.63
592952-92952101.442101.78
690480-9048098.74499.07
20min189997-8999798.21798.602.0198.7199.092.01
288396-8839696.47096.95
391551-9155199.913100.41
488325-8832596.39296.87
592922-92922101.409101.91
690891-9089199.19399.69
30min190086-9008698.31498.441.9698.9799.091.96
288348-8834896.41797.06
391434-9143499.785100.45
488041-8804196.08296.73
592579-92579101.035101.71
690699-9069998.98399.64
45min189773-8977397.97398.282.0698.7999.102.06
288257-8825796.31897.12
391379-9137999.725100.56
487750-8775095.76596.57
592587-92587101.044101.89
690596-9059698.87199.70
极限189711-8971197.90597.902.1698.8998.882.15
287631-8763195.63596.60
390851-9085199.149100.15
487323-8732395.29996.26
592324-92324100.757101.77
690382-9038298.63799.63
比索洛尔氨氯地平片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)0
对照品批号100374-202106对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.201077071068591069951072771072031072080.31
214.191072671071691072180.07
单位质量响应值RSD%判断
7549.867555.880.06数据可信
供试品溶液-2024021621批-氨氯地平-0.005hcl
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1108151-10815192.82492.911.9792.8292.911.97
2108120-10812092.79892.80
3108010-10801092.70392.70
4111857-11185796.00596.01
5105179-10517990.27390.27
6108166-10816692.83792.84
10min1115054-11505498.74998.910.8898.9099.060.89
2114497-11449798.27198.43
3114974-11497498.68098.83
4117102-117102100.507100.67
5114273-11427398.07998.23
6115520-11552099.14999.30
15min1114237-11423798.04898.600.8798.3798.920.87
2114467-11446798.24598.56
3114421-11442198.20698.52
4116860-116860100.299100.63
5114473-11447398.25098.56
6114834-11483498.56098.88
20min1113890-11389097.75098.190.9298.2398.670.93
2114122-11412297.94998.43
3113533-11353397.44497.93
4116412-11641299.915100.41
5113809-11380997.68098.16
6114616-11461698.37398.86
30min1113465-11346597.38598.101.0498.0398.741.04
2113271-11327197.21997.86
3114155-11415597.97798.62
4116519-116519100.006100.67
5113822-11382297.69298.33
6114546-11454698.31398.96
45min1113259-11325997.20898.150.9098.0298.960.90
2113662-11366297.55498.36
3113825-11382597.69498.50
4115993-11599399.555100.38
5114260-11426098.06898.87
6115124-11512498.80999.62
极限1113263-11326397.21297.441.0198.1898.411.01
2111871-11187196.01796.99
3112636-11263696.67497.64
4114881-11488198.60199.59
5114094-11409497.92598.89
6114399-11439998.18799.16
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