乌帕替尼缓释片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号240402对照品来源自制对照品使用方法直接使用
对照品含量(%)100.4对照品水分(%)0对照品稀释倍数1000
标示量(mg)15供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.971691751691581692791691381692881692080.05
214.981696891695871696380.05
单位质量响应值RSD%判断
11303.1411324.300.14数据可信
供试品溶液-24081401批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
30min124270-2427012.92313.042.3612.9213.042.37
224953-2495313.28613.29
323498-2349812.51212.51
424585-2458513.09013.09
525128-2512813.37913.38
624477-2447713.03313.03
60min142762-4276222.76923.041.4422.7923.061.45
243810-4381023.32723.35
342471-4247122.61422.63
443540-4354023.18323.20
544035-4403523.44623.47
642970-4297022.87922.90
120min169830-6983037.18137.531.6337.2437.591.63
271279-7127937.95338.01
368552-6855236.50136.56
470954-7095437.78037.84
571734-7173438.19538.26
670515-7051537.54637.61
240min1106855-10685556.89557.361.2557.0257.491.25
2108215-10821557.61957.74
3105805-10580556.33656.46
4108069-10806957.54157.66
5109781-10978158.45358.58
6107702-10770257.34657.47
360min1132465-13246570.53170.631.2370.7570.851.23
2131061-13106169.78470.00
3130760-13076069.62369.84
4133252-13325270.95071.17
5135177-13517771.97572.20
6133163-13316370.90371.12
480min1151097-15109780.45280.921.2780.7981.261.27
2152522-15252281.21181.55
3149527-14952779.61679.95
4151552-15155280.69481.03
5155334-15533482.70883.05
6151877-15187780.86781.20
600min1161351-16135185.91286.381.2686.3886.851.26
2162542-16254286.54687.02
3159642-15964285.00285.46
4162010-16201086.26286.73
5165851-16585188.30888.79
6162012-16201286.26486.73
720min1167587-16758789.23289.721.3289.8490.341.32
2168645-16864589.79590.41
3165574-16557488.16088.76
4167968-16796889.43590.05
5172313-17231391.74892.38
6168940-16894089.95290.57
960min1174451-17445192.88793.311.3693.6594.071.36
2175991-17599193.70794.47
3172248-17224891.71492.46
4174612-17461292.97293.74
5179399-17939995.52196.30
6174737-17473793.03993.80
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
1200min1176966-17696694.22694.851.3495.1495.771.34
2178826-17882695.21696.14
3175360-17536093.37194.27
4177700-17770094.61795.54
5182397-18239797.11898.06
6177583-17758394.55495.47
1440min1177124-17712494.31095.511.3695.3896.591.36
2179785-17978595.72796.81
3176945-17694594.21595.27
4179198-17919895.41496.49
5183670-18367097.79598.90
6179556-17955695.60596.68
乌帕替尼缓释片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号240402对照品来源自制对照品使用方法直接使用
对照品含量(%)100.4对照品水分(%)0对照品稀释倍数1000
标示量(mg)15供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.971697431698371699961699341698951698810.06
214.981700221700481700350.02
单位质量响应值RSD%判断
11348.1011350.800.02数据可信
供试品溶液-24081402批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
30min124416-2441612.95912.961.2412.9612.961.23
224262-2426212.87812.88
324742-2474213.13213.13
424527-2452713.01813.02
524673-2467313.09613.10
623918-2391812.69512.70
60min143403-4340323.03723.201.6523.0623.221.64
243699-4369923.19423.22
344352-4435223.54123.56
444186-4418623.45323.47
544195-4419523.45823.48
642443-4244322.52822.55
120min171443-7144337.92038.341.5737.9838.401.57
272398-7239838.42738.49
373078-7307838.78838.85
473093-7309338.79638.86
573060-7306038.77838.84
670333-7033337.33137.39
240min1112272-11227259.59160.061.6759.7160.181.67
2113831-11383160.41960.54
3113914-11391460.46360.59
4114475-11447560.76060.89
5114688-11468860.87361.00
6109726-10972658.24058.36
360min1141240-14124074.96774.772.2275.1974.992.22
2142760-14276075.77376.00
3141783-14178375.25575.48
4142905-14290575.85076.08
5141882-14188275.30775.53
6134613-13461371.44971.67
480min1162365-16236586.17986.021.4786.5386.371.47
2163003-16300386.51886.87
3162539-16253986.27286.62
4164103-16410387.10287.45
5162987-16298786.50986.86
6157375-15737583.53183.87
600min1173459-17345992.06891.771.6092.5692.261.60
2173619-17361992.15392.65
3172829-17282991.73392.23
4175769-17576993.29493.79
5174076-17407692.39592.89
6167635-16763588.97689.45
720min1179579-17957995.31694.951.4995.9695.601.49
2179575-17957595.31495.96
3179150-17915095.08895.74
4181830-18183096.51197.16
5179383-17938395.21295.86
6173839-17383992.26992.89
960min1185247-18524798.32498.051.5799.1398.861.57
2185286-18528698.34599.15
3185284-18528498.34499.15
4188032-18803299.803100.62
5185294-18529498.34999.16
6179280-17928095.15795.94
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
1200min1187106-18710699.31199.031.58100.28100.001.58
2187707-18770799.630100.60
3186970-18697099.239100.21
4189953-189953100.822101.80
5186677-18667799.083100.06
6181081-18108196.11397.05
1440min1187681-18768199.61699.151.58100.75100.281.58
2187744-18774499.650100.79
3187111-18711199.314100.45
4190081-190081100.890102.04
5186906-18690699.205100.34
6181277-18127796.21797.31
点击查看处理图标(自动生成)
　
原始图谱下载图谱(谢鑫慧 于 2024-08-18 10:43:48 完成)
生成报告数据部分下载报告(谢鑫慧 于 2024-08-18 10:44:11 完成)
Current page cost:53 ms