贝派度酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.19 3069523069793068333065653066143067890.07
210.153086833069553078190.40
单位质量响应值RSD%判断
30106.8730327.000.52数据可信
供试品溶液-24080801批-pH4.5(内含0.45%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
10min123597-235977.7878.266.877.798.266.87
226586-265868.7748.77
326289-262898.6768.68
423775-237757.8467.85
526871-268718.8688.87
623095-230957.6227.62
15min144268-4426814.60915.323.3014.6215.333.30
247921-4792115.81515.83
346503-4650315.34715.36
445108-4510814.88614.90
548165-4816515.89515.91
646476-4647615.33815.35
20min158676-5867619.36420.382.5619.4020.422.56
262673-6267320.68320.72
362385-6238520.58820.63
461796-6179620.39420.43
563024-6302420.79920.84
662033-6203320.47220.51
30min177212-7721225.48126.452.2925.5526.522.28
279371-7937126.19426.27
382021-8202127.06827.14
480374-8037426.52526.60
579814-7981426.34026.42
682120-8212027.10127.17
45min194525-9452531.19531.972.0831.3132.092.08
294730-9473031.26331.38
398133-9813332.38632.51
499394-9939432.80232.92
596225-9622531.75631.88
698207-9820732.41032.53
60min1103817-10381734.26134.931.6634.4335.101.65
2105782-10578234.91035.08
3106446-10644635.12935.30
4106918-10691835.28535.46
5103895-10389534.28734.46
6108275-10827535.73335.90
极限1117211-11721138.68239.032.1038.9039.252.09
2116205-11620538.35038.58
3118879-11887939.23239.46
4119385-11938539.39939.63
5115547-11554738.13338.36
6122291-12229140.35840.59
贝派度酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.19 3072423069063070383073993071303071430.07
210.153064903068153066520.08
单位质量响应值RSD%判断
30141.6130212.020.17数据可信
供试品溶液-24080801批-pH6.6
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min144665-4466514.76015.0016.3214.7615.0016.31
250005-5000516.52416.52
331926-3192610.55010.55
447352-4735215.64815.65
553571-5357117.70317.70
644838-4483814.81714.82
10min1163058-16305853.88353.604.0953.9153.624.10
2162472-16247253.68953.72
3149960-14996049.55549.57
4166810-16681055.12355.15
5169076-16907655.87255.90
6161794-16179453.46553.49
15min1228256-22825675.42875.361.0275.5475.471.03
2226472-22647274.83874.96
3224884-22488474.31474.41
4230539-23053976.18276.30
5230825-23082576.27776.40
6227290-22729075.10975.22
20min1253283-25328383.69883.720.5083.9483.960.51
2252085-25208583.30283.54
3253275-25327583.69583.92
4254597-25459784.13284.38
5254935-25493584.24484.49
6251844-25184483.22383.46
30min1272781-27278190.14190.130.5490.5290.510.53
2271508-27150889.72190.10
3274786-27478690.80491.17
4273054-27305490.23190.62
5273654-27365490.43090.82
6270764-27076489.47589.85
45min1280350-28035092.64292.710.6193.1793.240.60
2279779-27977992.45492.98
3283411-28341193.65494.17
4280451-28045192.67693.21
5281075-28107592.88293.42
6278258-27825891.95192.48
60min1281780-28178093.11593.100.5993.8093.780.59
2281037-28103792.86993.55
3284145-28414593.89794.57
4281791-28179193.11993.81
5282525-28252593.36194.06
6279146-27914692.24592.92
极限1279779-27977992.45492.620.6293.2993.460.61
2279784-27978492.45593.29
3282885-28288593.48094.31
4280551-28055192.70993.55
5281077-28107792.88393.73
6277663-27766391.75592.59
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