叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数25000
标示量(mg)0.4供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.391071901073801073241071361066371071330.28
210.381048711048921048820.02
单位质量响应值RSD%判断
10311.1610104.241.44数据可信
供试品溶液-24081903批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min126233-2623342.19241.712.5942.1941.722.59
226109-2610941.99341.99
325814-2581441.51841.52
426779-2677943.07043.07
525931-2593141.70641.71
624752-2475239.81039.81
10min138276-3827661.56262.631.5062.0363.091.49
238644-3864462.15462.62
338788-3878862.38562.85
439519-3951963.56164.04
539774-3977463.97164.43
638622-3862262.11862.56
15min144802-4480272.05873.332.1373.2174.492.11
245860-4586073.76074.92
345733-4573373.55574.71
445849-4584973.74274.93
547056-4705675.68376.86
644270-4427071.20272.33
20min148920-4892078.68178.482.0480.6380.452.03
248904-4890478.65580.63
348770-4877078.44080.41
448665-4866578.27180.28
550322-5032280.93682.95
647190-4719075.89977.82
30min152479-5247984.40584.411.6187.2387.261.61
252772-5277284.87787.73
352439-5243984.34187.18
452280-5228084.08586.96
553773-5377386.48689.40
651156-5115682.27785.04
45min154847-5484788.21488.101.2291.9891.881.23
255214-5521488.80492.60
354385-5438587.47191.25
454812-5481288.15891.97
555657-5565789.51793.39
653728-5372886.41490.10
60min156106-5610690.23989.591.8094.9894.351.79
256249-5624990.46995.25
355186-5518688.75993.51
456063-5606390.17094.96
556691-5669191.18096.05
653917-5391786.71891.36
90min156806-5680691.36590.331.2597.1196.091.24
256738-5673891.25597.04
355337-5533789.00294.74
456379-5637990.67896.47
556482-5648290.84496.73
655232-5523288.83394.44
极限156481-5648190.84290.151.5697.6196.921.53
256850-5685091.43598.24
355756-5575689.67696.40
456754-5675491.28198.08
555974-5597490.02696.92
654504-5450487.66294.25
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数25000
标示量(mg)0.4供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.391049761051341052551051121051641051280.10
210.381058511058451058480.01
单位质量响应值RSD%判断
10118.1910197.300.56数据可信
供试品溶液-24081904批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min120806-2080633.62535.503.1933.6335.503.18
222630-2263036.57336.57
322479-2247936.32936.33
421445-2144534.65834.66
522277-2227736.00336.00
622148-2214835.79435.79
10min133966-3396654.89456.121.8055.2756.511.80
235699-3569957.69458.10
334804-3480456.24856.65
434123-3412355.14755.53
534858-3485856.33556.74
634882-3488256.37456.77
15min141355-4135566.83566.642.8467.8267.662.82
242780-4278069.13870.19
341116-4111666.44967.48
439252-3925263.43664.43
541030-4103066.31067.34
641884-4188467.69068.71
20min145746-4574673.93272.962.4375.6674.722.41
246222-4622274.70176.52
344840-4484072.46774.23
443183-4318369.78971.49
545018-4501872.75574.52
645845-4584574.09275.87
30min150656-5065681.86781.012.7184.4183.582.67
250537-5053781.67484.32
349417-4941779.86482.44
447823-4782377.28879.77
551800-5180083.71686.29
650526-5052681.65784.26
45min153847-5384787.02485.222.2190.4888.682.19
254085-5408587.40890.96
351977-5197784.00287.46
451166-5116682.69186.03
552064-5206484.14287.64
653229-5322986.02589.53
60min154461-5446188.01687.351.7792.4491.761.77
255176-5517689.17293.70
353485-5348586.43990.83
452803-5280385.33789.59
553405-5340586.30990.75
654957-5495788.81893.28
90min156608-5660891.48689.482.0196.8994.871.98
255759-5575990.11495.63
355160-5516089.14694.50
453685-5368586.76291.97
554606-5460688.25093.65
656390-5639091.13496.58
极限155821-5582190.21489.411.5396.6395.791.51
256762-5676291.73598.25
354493-5449388.06894.41
454942-5494288.79394.96
554707-5470788.41494.79
655208-5520889.22395.69
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