磷酸奥司他韦干混悬项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号101096-202103对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.7对照品水分(%)0对照品稀释倍数100
标示量(mg)75供试品稀释倍数1系数0.7612
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.101554138155209115550421555580155524115544180.10
210.061564004155630015601520.35
单位质量响应值RSD%判断
153902.77155084.690.55数据可信
供试品溶液-B8086B03U1批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11657107-165710797.68497.350.8597.6897.350.85
21641384-164138496.75796.76
31644745-164474596.95596.95
41674284-167428498.69698.70
51635300-163530096.39896.40
61656238-165623897.63297.63
10min11679562-167956299.00798.270.8999.1798.430.89
21655114-165511497.56697.73
31662014-166201497.97398.13
41685789-168578999.37499.54
51647406-164740697.11297.27
61672034-167203498.56398.73
15min11679331-167933198.99498.280.9699.3298.600.97
21656687-165668797.65997.98
31659520-165952097.82698.15
41689578-168957899.59899.93
51646170-164617097.03997.36
61671740-167174098.54698.87
20min11675927-167592798.79398.020.8499.2998.510.84
21655261-165526197.57598.06
31655169-165516997.56998.06
41680556-168055699.06699.56
51644032-164403296.91397.40
61665889-166588998.20198.69
30min11672163-167216398.57197.880.9499.2398.530.93
21648889-164888997.19997.85
31651212-165121297.33697.99
41683328-168332899.22999.89
51643096-164309696.85897.50
61663935-166393598.08698.74
极限11670136-167013698.45297.560.9299.2798.370.92
21643054-164305496.85597.67
31648555-164855597.17997.99
41672581-167258198.59699.42
51634982-163498296.37997.19
61660525-166052597.88598.70
磷酸奥司他韦干混悬项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号101096-202103对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.7对照品水分(%)0对照品稀释倍数100
标示量(mg)75供试品稀释倍数1系数0.7612
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.101554833155568515569301556463155560615559030.06
210.061562896155721515600560.26
单位质量响应值RSD%判断
154049.80155075.150.47数据可信
供试品溶液-B8086B03U1批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11648863-164886397.15496.611.5097.1596.621.50
21672200-167220098.52998.53
31646058-164605896.98996.99
41646679-164667997.02597.03
51623481-162348195.65895.66
61600951-160095194.33194.33
10min11674259-167425998.65097.731.5198.8197.891.52
21693639-169363999.79299.96
31656803-165680397.62297.78
41659564-165956497.78497.95
51647983-164798397.10297.26
61619297-161929795.41295.57
15min11676546-167654698.78597.901.7399.1198.221.73
21706431-1706431100.546100.88
31656832-165683297.62397.95
41660780-166078097.85698.18
51647736-164773697.08897.41
61620615-162061595.49095.81
20min11668723-166872398.32497.701.5598.8298.191.55
21698075-1698075100.054100.55
31658680-165868097.73298.22
41657301-165730197.65198.14
51645859-164585996.97797.46
61620315-162031595.47295.95
30min11666315-166631598.18297.441.5198.8498.091.51
21691437-169143799.662100.33
31649807-164980797.21097.86
41657034-165703497.63598.29
51639956-163995696.62997.27
61617891-161789195.32995.96
极限11664919-166491998.10096.761.7598.9297.571.75
21685638-168563899.321100.15
31630135-163013596.05096.86
41639190-163919096.58497.40
51627703-162770395.90796.71
61605687-160568794.61095.40
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