依折麦布片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号ZT-705-231101-1-D对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.323368143363113367973372843367003367810.11
210.233369753367453368600.05
单位质量响应值RSD%判断
32633.8232928.640.64数据可信
供试品溶液-23110902批-pH4.5(内含%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1185779-18577956.67462.8914.6956.6762.9014.69
2158909-15890948.47748.48
3237776-23777672.53672.54
4233743-23374371.30571.31
5218768-21876866.73766.74
6202031-20203161.63161.63
10min1276984-27698484.49692.605.6384.6792.795.64
2293537-29353789.54689.69
3323341-32334198.63898.86
4318729-31872997.23197.44
5308147-30814794.00394.20
6300610-30061091.70491.89
15min1298101-29810190.93896.803.4991.3697.263.50
2318363-31836397.11997.53
3330603-330603100.853101.37
4323204-32320498.59699.10
5320598-32059897.80198.28
6313036-31303695.49495.95
20min1302910-30291092.40597.152.9293.1097.912.94
2319715-31971597.53298.24
3330338-330338100.773101.59
4322372-32237298.34299.14
5321544-32154498.09098.87
6313912-31391295.76296.51
30min1307619-30761993.84297.412.4294.8298.462.44
2320069-32006997.64098.64
3330333-330333100.771101.89
4322046-32204698.24399.34
5321537-32153798.08899.16
6314285-31428595.87596.91
45min1311297-31129794.96497.722.0096.2299.062.02
2322092-32209298.25799.55
3329976-329976100.662102.08
4321576-32157698.10099.49
5321499-32149998.07699.44
6315567-31556796.26697.59
60min1310077-31007794.59297.542.0196.1399.182.04
2320330-32033097.71999.31
3329464-329464100.506102.23
4321324-32132498.02399.71
5321254-32125498.00199.66
6316088-31608896.42598.04
极限1336795-336795102.742102.300.58104.57104.230.58
2331628-331628101.166103.04
3336192-336192102.558104.58
4335556-335556102.364104.34
5335269-335269102.277104.23
6336689-336689102.710104.61
依折麦布片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号ZT-705-231101-1-D对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.323376733368803371273364893367493369840.14
210.233363443360643362040.06
单位质量响应值RSD%判断
32653.4932864.520.46数据可信
供试品溶液-23120101批-pH4.5(内含%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1205108-20510862.61258.2315.9762.6158.2315.96
2155784-15578447.55547.56
3147798-14779845.11745.12
4208799-20879963.73963.74
5214136-21413665.36865.37
6212853-21285364.97664.98
10min1298799-29879991.21287.487.9691.4087.657.96
2266030-26603081.20981.35
3273253-27325383.41483.55
4263498-26349880.43680.63
5296214-29621490.42390.62
6321556-32155698.15998.35
15min1316555-31655596.63293.855.7797.0994.295.78
2297041-29704190.67691.06
3302625-30262592.38092.77
4280514-28051485.63086.06
5317433-31743396.90097.37
6330498-330498100.889101.38
20min1319963-31996397.67395.154.8298.4295.864.82
2303061-30306192.51393.17
3309741-30974194.55295.22
4287581-28758187.78888.48
5319966-31996697.67498.43
6329785-329785100.671101.46
30min1320516-32051697.84296.184.0998.8997.184.10
2308134-30813494.06295.00
3313909-31390995.82596.77
4294284-29428489.83490.79
5322104-32210498.32699.38
6331416-331416101.169102.26
45min1320277-32027797.76996.333.5099.1197.623.52
2309147-30914794.37195.59
3314737-31473796.07797.31
4297886-29788690.93492.16
5322104-32210498.32699.67
6329281-329281100.517101.91
60min1320101-32010197.71596.223.3099.3597.803.33
2308530-30853094.18395.68
3313826-31382695.79997.32
4298976-29897691.26692.76
5321972-32197298.28699.93
6327896-327896100.094101.79
极限1335099-335099102.293102.910.61104.22104.780.66
2337061-337061102.892104.68
3335670-335670102.468104.28
4336405-336405102.692104.46
5337570-337570103.048104.98
6340866-340866104.054106.05
依折麦布片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号ZT-705-231101-1-D对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.323364903371593370383371133369823369560.08
210.233374943373053374000.04
单位质量响应值RSD%判断
32650.7832981.430.72数据可信
供试品溶液-23120102批-pH4.5(内含%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1192752-19275258.73957.3510.0158.7457.3510.01
2199308-19930860.73660.74
3191103-19110358.23658.24
4167294-16729450.98150.98
5165070-16507050.30350.30
6213662-21366265.11165.11
10min1306967-30696793.54487.345.6293.7287.515.61
2304420-30442092.76892.95
3278227-27822784.78684.96
4286422-28642287.28387.44
5276939-27693984.39384.54
6266642-26664281.25581.45
15min1326089-32608999.37196.085.2699.8396.515.23
2319721-31972197.43197.89
3314419-31441995.81596.24
4329502-329502100.411100.83
5318597-31859797.08897.49
6283344-28334486.34586.78
20min1330748-330748100.79198.424.87101.5599.144.85
2321994-32199498.12398.88
3326163-32616399.394100.11
4336871-336871102.657103.37
5329479-329479100.404101.10
6292502-29250289.13689.83
30min1330304-330304100.65699.493.99101.71100.513.97
2321063-32106397.84098.89
3331676-331676101.074102.09
4339393-339393103.425104.45
5333625-333625101.668102.66
6302823-30282392.28193.25
45min1334264-334264101.86299.923.51103.22101.243.49
2321227-32122797.88999.23
3332315-332315101.268102.59
4338163-338163103.051104.38
5333841-333841101.733103.04
6307560-30756093.72594.97
60min1332879-332879101.44099.943.42103.11101.563.40
2319802-31980297.45599.09
3332684-332684101.381103.00
4337564-337564102.868104.51
5335863-335863102.350103.96
6308963-30896394.15295.68
极限1335019-335019102.092102.310.51104.06104.220.52
2338565-338565103.173105.10
3335031-335031102.096104.02
4336933-336933102.676104.63
5334003-334003101.783103.70
6334763-334763102.014103.82
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