依折麦布片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号ZT-705-231101-1-D对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.323350573365013373683369813372243366260.28
210.233365353366323365840.03
单位质量响应值RSD%判断
32618.8032901.660.62数据可信
供试品溶液-W024614批-pH4.5(内含%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1194024-19402459.22759.983.1259.2359.983.12
2207421-20742163.31663.32
3189608-18960857.87957.88
4198305-19830560.53360.53
5196507-19650759.98559.98
6193123-19312358.95258.95
10min1308933-30893394.30392.834.4694.4893.014.45
2315422-31542296.28496.47
3306918-30691893.68893.86
4280432-28043285.60385.78
5296795-29679590.59890.78
6316172-31617296.51396.69
15min1315444-31544496.29095.233.8096.7595.693.80
2320671-32067197.88698.36
3316764-31676496.69397.15
4290306-29030688.61789.06
5306906-30690693.68494.14
6321817-32181798.23698.70
20min1315439-31543996.28995.353.4997.0496.103.49
2320813-32081397.92998.70
3316504-31650496.61497.36
4292560-29256089.30590.01
5307613-30761393.90094.63
6321326-32132698.08698.85
30min1315931-31593196.43995.453.2897.4896.483.28
2320859-32085997.94399.01
3316072-31607296.48297.52
4294128-29412889.78490.76
5307996-30799694.01795.03
6321082-32108298.01299.07
45min1315688-31568896.36595.403.1397.6996.713.13
2319915-31991597.65599.02
3315390-31539096.27497.60
4294747-29474789.97391.21
5308441-30844194.15395.45
6320923-32092397.96399.31
60min1315296-31529696.24595.293.0497.8696.893.04
2319414-31941497.50299.16
3314753-31475396.08097.69
4294984-29498490.04591.56
5308135-30813594.05995.64
6320363-32036397.79299.44
极限1328262-328262100.20399.701.16102.11101.591.18
2327410-32741099.943101.89
3328416-328416100.250102.15
4323091-32309198.625100.41
5321124-32112498.02499.89
6331295-331295101.129103.07
依折麦布片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号ZT-705-231101-1-D对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.323368663367703367633367563368253367960.02
210.233361853361563361700.01
单位质量响应值RSD%判断
32635.2732861.190.49数据可信
供试品溶液-W024614批-pH4.5(内含%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1114459-11445934.95249.9033.6334.9549.9033.62
2203137-20313762.03162.03
383133-8313325.38625.39
4206448-20644863.04263.04
5216139-21613966.00166.00
6157091-15709147.97047.97
10min1279683-27968385.40587.3912.3985.5187.5412.42
2300920-30092091.89092.08
3217398-21739866.38566.46
4305173-30517393.18993.38
5312482-31248295.42195.62
6301521-30152192.07492.22
15min1308331-30833194.15392.688.3894.5193.098.42
2314963-31496396.17896.64
3252132-25213276.99277.27
4313837-31383795.83496.30
5319287-31928797.49997.98
6312491-31249195.42395.84
20min1310443-31044394.79893.536.7195.4494.226.77
2315680-31568096.39797.15
3264760-26476080.84881.35
4314693-31469396.09696.85
5318995-31899597.40998.19
6313204-31320495.64196.35
30min1313232-31323295.65094.005.8496.5894.975.89
2315386-31538696.30797.35
3271454-27145482.89283.64
4314993-31499396.18797.23
5318915-31891597.38598.45
6313040-31304095.59196.58
45min1314454-31445496.02394.484.7797.2495.734.84
2315706-31570696.40597.73
3279563-27956385.36886.37
4315399-31539996.31197.64
5318582-31858297.28398.64
6312622-31262295.46396.74
60min1314789-31478996.12594.694.3597.6396.234.42
2316058-31605896.51398.13
3282815-28281586.36187.62
4315424-31542496.31997.94
5318178-31817897.16098.81
6313348-31334895.68597.25
极限1332817-332817101.630100.291.20103.42102.111.10
2328076-328076100.182102.09
3332189-332189101.438102.95
4325692-32569299.454101.37
5329335-329335100.567102.51
6322507-32250798.482100.34
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