依折麦布片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号ZT-705-231101-1-D对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.323366863368703368133365663370723368010.06
210.233371243374983373110.08
单位质量响应值RSD%判断
32635.7632972.730.73数据可信
供试品溶液-W027854批-pH4.5(内含%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1191531-19153158.38848.0322.6058.3948.0422.60
2175614-17561453.53553.54
3104839-10483931.96031.96
4191099-19109958.25658.26
5155561-15556147.42247.42
6126737-12673738.63538.64
10min1320842-32084297.80888.9311.3397.9889.0711.34
2320913-32091397.82997.99
3258439-25843978.78478.88
4322219-32221998.22798.40
5273222-27322283.29183.43
6254657-25465777.63177.75
15min1324498-32449898.92297.372.7399.3997.782.77
2327673-32767399.890100.34
3313161-31316195.46695.80
4329304-329304100.387100.86
5309759-30975994.42994.82
6312066-31206695.13295.48
20min1322771-32277198.39698.971.8299.1699.681.81
2326707-32670799.596100.35
3326300-32630099.471100.09
4328523-328523100.149100.92
5313707-31370795.63396.31
6329988-329988100.596101.23
30min1322275-32227598.24499.152.1799.31100.152.14
2326006-32600699.382100.43
3328820-328820100.240101.16
4328168-328168100.041101.11
5312914-31291495.39196.35
6333308-333308101.608102.54
45min1324197-32419798.83099.422.23100.19100.722.21
2325885-32588599.345100.70
3330296-330296100.690101.91
4329324-329324100.393101.76
5313048-31304895.43296.68
6334000-334000101.819103.06
60min1324500-32450098.92399.392.26100.57100.982.23
2325356-32535699.184100.83
3330355-330355100.708102.23
4329336-329336100.397102.07
5312763-31276395.34596.88
6333830-333830101.767103.31
极限1332042-332042101.222102.031.13103.17103.931.12
2334506-334506101.973103.92
3339111-339111103.377105.20
4337578-337578102.910104.88
5328839-328839100.245102.07
6336135-336135102.470104.32
依折麦布片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号ZT-705-231101-1-D对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.323374373371363367993370023373503371450.08
210.233354963356803355880.04
单位质量响应值RSD%判断
32669.0932804.300.30数据可信
供试品溶液-W027854批-pH4.5(内含%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1106590-10659032.56035.8235.8132.5635.8235.81
298501-9850130.08930.09
397491-9749129.78029.78
493727-9372728.63128.63
5104842-10484232.02632.03
6202418-20241861.83261.83
10min1230385-23038570.37577.785.5170.4777.885.52
2249836-24983676.31776.41
3253529-25352977.44577.53
4261279-26127979.81379.90
5261251-26125179.80479.90
6271381-27138182.89883.08
15min1272019-27201983.09392.095.9683.4092.435.92
2311687-31168795.21195.53
3312625-31262595.49795.82
4310975-31097594.99395.32
5315285-31528596.31096.65
6286251-28625187.44187.87
20min1294791-29479190.04997.215.9590.6197.835.91
2329336-329336100.602101.21
3329014-329014100.504101.11
4331318-331318101.207101.82
5332046-332046101.430102.05
6292915-29291589.47690.17
30min1315656-31565696.42399.764.9397.25100.674.88
2335457-335457102.472103.38
3334213-334213102.092103.00
4337982-337982103.243104.16
5337644-337644103.140104.07
6298525-29852591.19092.16
45min1325248-32524899.353100.584.58100.47101.784.53
2336661-336661102.839104.05
3335172-335172102.385103.60
4338726-338726103.470104.69
5339396-339396103.675104.91
6300314-30031491.73792.98
60min1326011-32601199.586100.544.42101.00102.054.37
2336377-336377102.753104.28
3334322-334322102.125103.65
4338088-338088103.275104.81
5338924-338924103.531105.08
6301007-30100791.94893.46
极限1332201-332201101.477102.850.83103.19104.660.87
2337568-337568103.117104.95
3336627-336627102.829104.66
4339435-339435103.687105.53
5339348-339348103.660105.52
6334942-334942102.314104.10
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