替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.612679926574267932705026871268170.64
214.432674926899268240.40
单位质量响应值RSD%判断
1835.521858.910.90数据可信
供试品溶液-2024070321批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min125819-2581998.05996.262.6498.0696.262.64
225017-2501795.01395.01
324821-2482194.26994.27
426369-26369100.148100.15
525461-2546196.69996.70
624591-2459193.39593.40
10min126322-2632299.969100.092.47100.95101.052.47
226029-2602998.85799.81
325535-2553596.98097.92
427474-27474104.345105.35
526569-26569100.907101.87
626190-2619099.468100.40
15min126191-2619199.472100.432.61101.45102.392.60
226211-2621199.548101.49
325773-2577397.88499.80
427769-27769105.465107.51
526488-26488100.600102.58
626224-2622499.597101.53
20min126204-2620499.521100.421.86102.50103.381.87
226429-26429100.376103.31
325688-2568897.562100.45
427168-27168103.182106.28
526679-26679101.325104.31
626470-26470100.531103.46
30min126100-2610099.126100.152.06103.10104.122.06
226406-26406100.288104.23
325507-2550796.874100.74
427123-27123103.012107.14
526656-26656101.238105.23
626423-26423100.353104.28
极限126106-2610699.14998.831.07104.11103.811.08
226144-2614499.293104.23
325464-2546496.711101.55
426090-2609099.088104.25
526195-2619599.487104.49
626140-2614099.278104.21
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.612684626990268502696126888269070.25
214.432697627026270010.14
单位质量响应值RSD%判断
1841.681871.171.13数据可信
供试品溶液-ald批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min125287-2528795.56492.531.8595.5692.521.84
224297-2429791.82391.82
324748-2474893.52793.53
424222-2422291.53991.54
524209-2420991.49091.49
624135-2413591.21091.21
10min125185-2518595.17996.161.2096.1397.091.18
225139-2513995.00595.92
325781-2578197.43198.37
425586-2558696.69497.61
525775-2577597.40898.32
625209-2520995.26996.18
15min125070-2507094.74495.072.7296.6596.962.68
224364-2436492.07693.94
325836-2583697.63999.55
424403-2440392.22394.11
525957-2595798.09699.99
625313-2531395.66297.53
20min124379-2437992.13394.432.4394.9997.272.38
224163-2416391.31694.11
325513-2551396.41899.30
424904-2490494.11796.92
525550-2555096.55899.43
625411-2541196.03398.85
30min125049-2504994.66595.061.3298.4498.841.28
224891-2489194.06897.77
324759-2475993.56997.42
425131-2513194.97598.72
525559-2555996.592100.43
625537-2553796.509100.29
极限124654-2465493.17294.601.6697.8999.341.62
224706-2470693.36898.01
325276-2527695.523100.31
425170-2517095.12299.82
525682-2568297.057101.86
624707-2470793.37298.12
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.612691026874267542671326634267770.43
214.432651926578265480.16
单位质量响应值RSD%判断
1832.791839.780.27数据可信
供试品溶液-2024070421批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min126199-26199100.09198.432.93100.0998.432.93
225898-2589898.94198.94
324884-2488495.06795.07
426280-26280100.400100.40
524778-2477894.66294.66
626553-26553101.443101.44
10min126426-26426100.958101.452.56101.96102.432.56
226530-26530101.356102.34
326110-2611099.751100.70
427104-27104103.548104.55
525629-2562997.91398.86
627522-27522105.145106.16
15min126609-26609101.657101.671.46103.67103.671.48
226670-26670101.890103.89
326335-26335100.611102.56
426626-26626101.722103.76
526150-2615099.904101.83
627289-27289104.255106.32
20min126422-26422100.943101.613.10103.97104.623.07
226913-26913102.819105.84
326482-26482101.172104.13
426686-26686101.952105.01
525263-2526396.51599.44
627807-27807106.234109.34
30min126224-26224100.187100.462.02104.22104.502.03
226398-26398100.851104.90
326199-26199100.091104.06
426183-26183100.030104.11
525565-2556597.669101.56
627208-27208103.946108.12
极限125904-2590498.96499.032.46104.00104.072.43
225270-2527096.542101.60
326001-2600199.335104.30
426327-26327100.580105.66
525173-2517396.171101.04
626857-26857102.605107.82
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