叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.391054841055551055141055531056341055480.06
210.381050941053281052110.16
单位质量响应值RSD%判断
10158.6110135.930.16数据可信
供试品溶液-24081904批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min117215-1721527.85027.254.4127.8527.254.40
217358-1735828.08128.08
317258-1725827.92027.92
417451-1745128.23228.23
515980-1598025.85225.85
615815-1581525.58525.59
10min128037-2803745.35846.242.5845.6746.542.58
229059-2905947.01147.32
328564-2856446.21046.52
429643-2964347.95648.27
527550-2755044.57044.86
628633-2863346.32246.61
15min134866-3486656.40557.521.6457.2258.331.65
235767-3576757.86358.70
335511-3551157.44958.27
436424-3642458.92659.77
534956-3495656.55157.33
635799-3579957.91558.71
20min139534-3953463.95765.171.7365.4066.631.70
240930-4093066.21667.69
339603-3960364.06965.53
440745-4074565.91667.42
541044-4104466.40067.81
639847-3984764.46465.91
30min145082-4508272.93372.701.5275.0874.881.51
245930-4593074.30476.52
344669-4466972.26474.44
445269-4526973.23575.47
543885-4388570.99673.14
644786-4478672.45474.61
45min148986-4898679.24879.241.0082.2182.230.99
249689-4968980.38683.42
349229-4922979.64282.62
448820-4882078.98082.03
548211-4821177.99580.93
648968-4896879.21982.18
60min151829-5182983.84882.901.0787.6986.771.04
251523-5152383.35387.28
351323-5132383.02986.89
450932-5093282.39786.32
550315-5031581.39885.20
651543-5154383.38587.23
90min153503-5350386.55686.460.7191.3391.250.70
253305-5330586.23691.09
353790-5379087.02091.80
453665-5366586.81891.66
552752-5275285.34190.05
653648-5364886.79091.56
极限153925-5392587.23987.101.0592.9792.850.98
253246-5324686.14091.96
354557-5455788.26194.01
453439-5343986.45292.26
553406-5340686.39992.06
654448-5444888.08593.82
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.391302764130324613036251303239130298913031730.03
210.381304560130401313042860.03
单位质量响应值RSD%判断
125425.70125653.760.13数据可信
供试品溶液-24081902批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min199211-9921112.97313.134.3312.9713.134.33
2103242-10324213.50013.50
397458-9745812.74412.74
498426-9842612.87112.87
5107926-10792614.11314.11
696421-9642112.60812.61
10min1180123-18012323.55424.163.3523.7024.303.35
2190148-19014824.86425.01
3185740-18574024.28824.43
4183536-18353624.00024.14
5192801-19280125.21125.37
6176205-17620523.04123.18
15min1242835-24283531.75432.281.8532.1632.701.87
2248518-24851832.49732.92
3247621-24762132.38032.79
4248858-24885832.54232.95
5253039-25303933.08833.53
6240396-24039631.43531.83
20min1286850-28685037.51038.121.8338.2738.891.84
2290514-29051437.98938.78
3293149-29314938.33339.10
4294477-29447738.50739.28
5299260-29926039.13239.94
6284647-28464737.22137.97
30min1345888-34588845.23045.691.1146.4046.891.13
2346324-34632445.28746.50
3350374-35037445.81647.01
4352431-35243146.08547.28
5355230-35523046.45147.69
6346398-34639845.29646.46
45min1397009-39700951.91452.501.3253.5954.201.29
2397964-39796452.03953.75
3395732-39573251.74753.45
4408558-40855853.42455.14
5404902-40490252.94654.70
6404863-40486352.94154.60
60min1430018-43001856.23157.091.3758.4959.381.34
2432039-43203956.49558.79
3431534-43153456.42958.71
4442333-44233357.84160.15
5442357-44235757.84460.19
6441200-44120057.69359.94
90min1466436-46643660.99362.521.7963.8765.441.74
2474808-47480862.08865.01
3471658-47165861.67664.58
4486467-48646763.61266.56
5481212-48121262.92565.91
6487900-48790063.80066.69
极限1509362-50936266.60667.552.4770.1671.162.37
2525369-52536968.69972.31
3499711-49971165.34468.94
4535805-53580570.06473.72
5511515-51151566.88770.57
6517508-51750867.67171.27
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