诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.813866479386957938674683871390387304838695930.08
29.823899896389960638997510.01
单位质量响应值RSD%判断
394453.92397123.320.48数据可信
供试品溶液-240821批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min12760647-276064762.52558.8412.6862.5358.8512.68
23116804-311680470.59270.59
32637170-263717059.72859.73
42138979-213897948.44548.45
52448504-244850455.45555.46
62486711-248671156.32156.32
10min14299826-429982697.38691.245.2897.4991.345.28
24180135-418013594.67594.79
33976710-397671090.06790.17
43947101-394710189.39789.48
53686161-368616183.48783.58
64082027-408202792.45392.55
15min14527057-4527057102.53298.154.33102.8098.404.33
24487734-4487734101.641101.92
34329919-432991998.06798.32
44349373-434937398.50898.74
53996449-399644990.51490.75
64311443-431144397.64997.90
20min14578478-4578478103.69799.403.78104.1399.813.78
24468394-4468394101.203101.65
34477854-4477854101.418101.83
44417154-4417154100.043100.44
54121745-412174593.35293.73
64267867-426786796.66297.07
30min14582666-4582666103.791100.203.15104.40100.783.16
24512384-4512384102.200102.81
34477155-4477155101.402101.98
44448237-4448237100.747101.31
54199293-419929395.10995.65
64324127-432412797.93698.51
诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.813939320393203839404153940476393054039365580.13
29.823938300393544539368720.06
单位质量响应值RSD%判断
401280.12400903.460.07数据可信
供试品溶液-240821批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13736137-373613783.49988.686.8283.5088.686.82
23718039-371803983.09483.09
33783294-378329484.55384.55
44303914-430391496.18896.19
54287863-428786395.82995.83
63978208-397820888.90988.91
10min14467288-446728899.839101.242.3099.98101.392.29
24721532-4721532105.522105.66
34538394-4538394101.429101.57
44513042-4513042100.862101.02
54416060-441606098.69598.85
64524551-4524551101.119101.27
15min14507089-4507089100.729101.842.11101.03102.152.10
24736717-4736717105.861106.18
34550725-4550725101.704102.01
44550016-4550016101.688102.02
54453538-445353899.53299.86
64541906-4541906101.507101.82
20min14547634-4547634101.635102.062.07102.11102.552.06
24741291-4741291105.963106.45
34558204-4558204101.871102.35
44544650-4544650101.568102.07
54452049-445204999.49999.99
64556470-4556470101.833102.32
30min14555521-4555521101.811101.882.05102.45102.542.04
24718727-4718727105.459106.13
34544609-4544609101.567102.22
44558102-4558102101.869102.54
54427142-442714298.94299.60
64547353-4547353101.629102.28
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