叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.112462782464062464982463332464392463910.04
210.142465282462852464060.07
单位质量响应值RSD%判断
24371.0224300.390.21数据可信
供试品溶液-24082901批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min167160-6716045.30450.016.0145.3050.016.01
275451-7545150.89750.90
370595-7059547.62147.62
479276-7927653.47753.48
575307-7530750.80050.80
677011-7701151.94951.95
10min191436-9143661.68065.314.0062.1865.864.01
295521-9552164.43565.00
395044-9504464.11364.64
4100525-10052567.81168.40
596354-9635464.99765.56
6102013-10201368.81469.39
15min1103798-10379870.01972.052.0271.2173.332.06
2105931-10593171.45772.74
3106527-10652771.85973.10
4110210-11021074.34475.69
5106344-10634471.73673.02
6108049-10804972.88674.23
20min1110923-11092374.82575.921.1676.7978.001.21
2111953-11195375.52077.60
3112937-11293776.18378.22
4114341-11434177.13179.30
5111514-11151475.22477.31
6113566-11356676.60878.76
30min1120308-12030881.15680.482.0783.9583.402.04
2116666-11666678.69981.61
3118906-11890680.21083.10
4122750-12275082.80385.83
5116449-11644978.55381.47
6120761-12076181.46184.46
45min1122005-12200582.30081.761.4086.0085.581.37
2118662-11866280.04583.83
3122567-12256782.68086.46
4122575-12257582.68586.64
5119489-11948980.60384.40
6121934-12193482.25386.16
60min1122513-12251382.64381.451.2887.2686.181.23
2119919-11991980.89385.57
3121090-12109081.68386.38
4120672-12067281.40186.27
5118231-11823179.75584.44
6122040-12204082.32487.15
90min1121695-12169582.09181.420.9687.6287.060.93
2120081-12008181.00386.58
3121681-12168182.08287.69
4120891-12089181.54987.32
5118681-11868180.05885.63
6121215-12121581.76787.50
极限1120724-12072481.43680.401.0887.8886.931.02
2119364-11936480.51987.00
3119290-11929080.46986.98
4119159-11915980.38187.06
5116833-11683378.81285.28
6119717-11971780.75787.40
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.112462912461602464272466202461102463220.09
210.142462162458332460240.12
单位质量响应值RSD%判断
24364.1924262.720.30数据可信
供试品溶液-24082902批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min153521-5352136.13733.039.5236.1433.039.52
244317-4431729.92229.92
345930-4593031.01131.01
450891-5089134.36134.36
554554-5455436.83436.83
644292-4429229.90529.91
10min172384-7238448.87345.606.6249.2745.976.64
264199-6419943.34643.68
364557-6455743.58843.93
468862-6886246.49546.88
572825-7282549.17049.58
662388-6238842.12342.46
15min181903-8190355.30052.735.7456.2453.605.77
275105-7510550.71051.52
375845-7584551.20952.04
478612-7861253.07853.98
584512-8451257.06158.02
672591-7259149.01249.81
20min188035-8803559.44056.984.7061.0058.444.75
279657-7965753.78355.16
382059-8205955.40556.80
484490-8449057.04658.53
590049-9004960.80062.39
682082-8208255.42056.77
30min193343-9334363.02462.462.3465.2464.552.43
290570-9057061.15163.13
392556-9255662.49264.51
491608-9160861.85263.97
596306-9630665.02467.29
690627-9062761.19063.15
45min196907-9690765.43065.072.9768.3567.863.04
294964-9496464.11866.77
394179-9417963.58866.30
496599-9659965.22268.03
5101648-10164868.63171.62
693974-9397463.45066.09
60min1112310-11231075.83068.056.2679.4871.566.13
297466-9746665.80869.17
396659-9665965.26368.68
497914-9791466.11069.64
5104025-10402570.23673.99
696375-9637565.07168.42
90min1102228-10222869.02368.552.8673.5172.822.93
298530-9853066.52670.62
3100653-10065367.95972.10
4100312-10031267.72972.00
5106943-10694372.20676.74
6100541-10054167.88471.95
极限1104129-10412970.30669.852.7875.5674.882.86
2101379-10137968.45073.29
3102347-10234769.10374.00
4102892-10289269.47174.49
5108884-10888473.51778.85
6101130-10113068.28173.10
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.112463502464102464982464912466992464900.06
210.142478252477412477830.03
单位质量响应值RSD%判断
24380.8124436.190.17数据可信
供试品溶液-24082903批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min160675-6067540.80740.622.3440.8140.622.34
260230-6023040.50840.51
358438-5843839.30339.30
462284-6228441.88941.89
561473-6147341.34441.34
659256-5925639.85339.85
10min177817-7781752.33652.751.3752.7953.201.37
277067-7706751.83252.28
377902-7790252.39352.83
479736-7973653.62754.09
579654-7965453.57254.03
678437-7843752.75353.20
15min186768-8676858.35658.771.3259.3959.801.30
285534-8553457.52658.55
387797-8779759.04860.07
487136-8713658.60459.66
588408-8840859.45960.51
688620-8862059.60260.63
20min192012-9201261.88362.072.1663.5763.762.11
288894-8889459.78661.45
394076-9407663.27164.95
491363-9136361.44663.16
593981-9398163.20764.92
693385-9338562.80664.50
30min197100-9710065.30565.191.3067.6867.571.26
296274-9627464.74967.08
399147-9914766.68269.06
495791-9579164.42566.82
597335-9733565.46367.88
695903-9590364.50066.89
45min199914-9991467.19867.581.8070.2970.681.74
298338-9833866.13869.19
3103211-10321169.41572.53
498945-9894566.54669.66
5100854-10085467.83070.97
6101654-10165468.36871.47
60min1103232-10323269.42969.041.8173.2772.901.76
2100103-10010367.32571.11
3105778-10577871.14175.03
4101903-10190368.53572.39
5102438-10243868.89572.79
6102463-10246368.91272.78
90min1105490-10549070.94870.631.3075.5675.251.27
2103731-10373169.76574.30
3107390-10739072.22676.91
4104246-10424670.11174.72
5105264-10526470.79675.46
6103969-10396969.92574.56
极限1106840-10684071.85671.251.4277.2676.661.37
2104970-10497070.59875.90
3108612-10861273.04778.53
4105390-10539070.88076.27
5104970-10497070.59876.05
6104854-10485470.52075.93
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