叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.111230416123118512310871231023123060712308640.03
210.141230108123006512300860.01
单位质量响应值RSD%判断
121747.18121310.260.26数据可信
供试品溶液-24082904批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1115232-11523215.56515.795.5015.5715.795.50
2120000-12000016.21016.21
3126061-12606117.02817.03
4110123-11012314.87514.88
5120154-12015416.23016.23
6109602-10960214.80514.80
10min1214048-21404828.91429.283.4629.0929.463.46
2221718-22171829.95030.13
3224120-22412030.27430.46
4222982-22298230.12030.29
5212828-21282828.74928.93
6204912-20491227.67927.84
15min1277593-27759337.49737.504.2637.9938.004.23
2287779-28777938.87339.39
3288355-28835538.95139.48
4257590-25759034.79535.30
5283408-28340838.28338.78
6270884-27088436.59137.06
20min1317562-31756242.89643.804.5043.8144.724.47
2338071-33807145.66746.61
3335079-33507945.26246.22
4300225-30022540.55441.44
5334898-33489845.23846.16
6319790-31979043.19744.08
30min1380878-38087851.44952.194.7252.8453.604.68
2403976-40397654.56956.02
3395319-39531953.40054.86
4354173-35417347.84249.18
5400408-40040854.08755.51
6383507-38350751.80453.16
45min1434162-43416258.64660.165.3060.6162.155.24
2463116-46311662.55864.62
3449989-44998960.78462.84
4404618-40461854.65656.52
5470704-47070463.58365.61
6449798-44979860.75962.69
60min1469334-46933463.39765.485.7666.0168.135.67
2507168-50716868.50871.26
3487357-48735765.83268.56
4437770-43777059.13461.61
5514248-51424869.46472.20
6492582-49258266.53869.15
90min1503435-50343568.00470.525.2171.3273.905.10
2553287-55328774.73878.25
3532648-53264871.95075.41
4485035-48503565.51868.65
5509267-50926768.79272.30
6548869-54886974.14177.49
极限1583954-58395478.88079.421.9082.9583.581.94
2594925-59492580.36284.71
3576095-57609577.81982.08
4574767-57476777.63981.50
5599337-59933780.95885.23
6598525-59852580.84985.02
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.111229652122995212300831229710122984812298490.02
210.141224820122575512252880.06
单位质量响应值RSD%判断
121646.79120837.080.48数据可信
供试品溶液-24082905批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1103180-10318013.97115.325.6813.9715.325.67
2111002-11100215.03015.03
3116417-11641715.76315.76
4122618-12261816.60316.60
5113872-11387215.41815.42
6111954-11195415.15915.16
10min1188387-18838725.50826.532.9225.6626.702.95
2191043-19104325.86726.03
3198784-19878426.91527.09
4203863-20386327.60327.79
5198957-19895726.93927.11
6194382-19438226.31926.49
15min1258765-25876535.03734.983.1635.4835.453.15
2244515-24451533.10733.56
3255638-25563834.61335.09
4267106-26710636.16636.66
5265838-26583835.99536.47
6258270-25827034.97035.43
20min1301515-30151540.82540.773.5541.6541.623.52
2284205-28420538.48139.30
3294594-29459439.88840.75
4306181-30618141.45742.35
5315270-31527042.68843.56
6304871-30487141.28042.13
30min1364447-36444749.34649.432.8150.6350.742.81
2347290-34729047.02348.27
3362058-36205849.02350.32
4367009-36700949.69351.05
5376726-37672651.00952.35
6372873-37287350.48751.80
45min1419880-41988056.85257.381.7258.6859.231.73
2414045-41404556.06257.83
3428577-42857758.02959.88
4421891-42189157.12459.03
5435021-43502158.90260.81
6423113-42311357.29059.16
60min1460620-46062062.36862.630.9764.8365.130.98
2457910-45791062.00164.40
3465512-46551263.03065.52
4457488-45748861.94464.48
5467175-46717563.25665.82
6466807-46680763.20665.71
90min1502457-50245768.03369.132.0371.1972.322.01
2501737-50173767.93571.02
3515064-51506469.74072.93
4503113-50311368.12271.35
5528203-52820371.51974.79
6512766-51276669.42972.64
极限1565877-56587776.62077.211.6080.5381.161.57
2565268-56526876.53780.38
3571605-57160577.39581.36
4557620-55762075.50279.49
5580470-58047078.59682.66
6580436-58043678.59182.57
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