叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数25000
标示量(mg)0.4供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.119907898748984759833998124985530.38
210.149697097054970120.07
单位质量响应值RSD%判断
9748.079567.261.33数据可信
供试品溶液-24082906批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min122970-2297039.04837.982.5339.0537.982.53
222092-2209237.55537.56
321692-2169236.87536.88
422479-2247938.21338.21
522994-2299439.08839.09
621823-2182337.09837.10
10min133115-3311556.29357.422.1556.7357.842.13
234920-3492059.36259.78
333458-3345856.87757.29
434275-3427558.26558.69
533048-3304856.18056.61
633856-3385657.55357.97
15min140743-4074369.26168.202.6270.3269.262.58
241033-4103369.75470.83
339568-3956867.26368.30
439598-3959867.31468.39
538539-3853965.51466.57
641219-4121970.07071.12
20min145910-4591078.04475.792.4579.8777.602.42
245364-4536477.11678.97
343666-4366674.23076.02
443819-4381974.49076.31
543358-4335873.70675.49
645373-4537377.13178.96
30min149625-4962584.35983.502.0187.0686.161.99
250152-5015285.25587.96
348256-4825682.03284.65
448465-4846582.38885.04
548030-4803081.64884.25
650189-5018985.31888.01
45min153593-5359391.10589.692.0794.7493.282.05
253355-5335590.70094.36
352079-5207988.53192.06
452973-5297390.05193.61
550880-5088086.49390.01
653690-5369091.27094.90
60min154918-5491893.35792.701.5698.0097.291.55
254580-5458092.78397.45
353430-5343090.82895.34
454950-5495093.41297.98
553657-5365791.21495.69
655662-5566294.62299.27
90min156718-5671896.41795.481.87102.10101.091.82
255569-5556994.464100.16
354593-5459392.80598.32
457534-5753497.804103.41
555800-5580094.857100.34
656773-5677396.511102.21
极限161454-61454104.46896.684.22111.22103.364.01
256326-5632695.751102.50
354345-5434592.38398.93
456859-5685996.657103.35
556051-5605195.283101.82
656215-5621595.562102.34
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数25000
标示量(mg)0.4供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.119887098708987579892598960988440.11
210.149755997697976280.10
单位质量响应值RSD%判断
9776.859628.011.09数据可信
供试品溶液-24082907批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min119300-1930032.65634.182.5532.6634.182.55
219976-1997633.80033.80
320339-2033934.41534.41
420595-2059534.84834.85
520734-2073435.08335.08
620262-2026234.28434.28
10min130356-3035651.36453.622.4551.7354.002.44
231399-3139953.12953.50
331889-3188953.95854.34
432015-3201554.17154.56
531808-3180853.82154.21
632677-3267755.29155.67
15min136545-3654561.83664.532.7262.7765.502.71
237906-3790664.13965.10
337824-3782464.00064.98
437985-3798564.27265.26
539160-3916066.26167.25
639397-3939766.66267.66
20min140909-4090969.22071.102.5870.8472.802.57
241687-4168770.53672.21
341463-4146370.15771.85
441333-4133369.93771.64
543592-4359273.76075.48
643150-4315073.01274.75
30min145346-4534676.72879.203.2879.1281.683.23
246670-4667078.96881.43
346362-4636278.44780.92
445570-4557077.10779.59
549560-4956083.85886.40
647331-4733180.08682.63
45min150048-5004884.68484.351.9687.9387.711.92
250323-5032385.14988.49
348979-4897982.87586.22
448393-4839381.88385.22
550349-5034985.19388.67
651013-5101386.31689.75
60min151117-5111786.49286.881.6290.6891.181.61
251997-5199787.98192.27
351042-5104286.36590.63
449989-4998984.58488.83
551629-5162987.35991.78
652317-5231788.52392.92
90min153356-5335690.28190.432.3795.4395.702.33
253298-5329890.18395.45
352394-5239488.65393.88
451819-5181987.68092.87
554926-5492692.93798.33
654865-5486592.83498.21
极限154883-5488392.86590.552.3199.0196.822.21
253911-5391191.22097.49
352247-5224788.40494.61
451775-5177587.60693.77
553860-5386091.13497.56
654421-5442192.08398.49
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