托伐普坦口崩片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号101242-201201对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数10000
标示量(mg)15供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.12 1979921978841970701963961954161969520.55
216.171976871978431977650.06
单位质量响应值RSD%判断
12217.8712230.360.08数据可信
供试品溶液-3G80SDA2批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min14376-43762.1482.1913.892.152.1913.96
25019-50192.4632.46
35206-52062.5552.56
43713-37131.8221.82
54666-46662.2902.29
63794-37941.8621.86
10min118315-183158.99010.367.609.0010.377.60
220762-2076210.19110.20
321622-2162210.61310.63
420885-2088510.25110.26
523075-2307511.32611.34
621967-2196710.78210.79
15min128271-2827113.87616.449.0213.9416.519.01
234825-3482517.09317.16
331834-3183415.62515.70
433776-3377616.57816.65
536247-3624717.79117.87
635974-3597417.65717.73
20min141170-4117020.20822.145.7320.3522.305.74
245980-4598022.56922.73
344297-4429721.74221.90
443678-4367821.43921.60
548198-4819823.65723.83
647304-4730423.21823.39
30min157283-5728328.11629.003.4328.3729.283.44
259869-5986929.38629.68
357781-5778128.36128.64
456942-5694227.94928.23
560772-6077229.82930.13
661810-6181030.33830.64
45min172357-7235735.51535.432.9035.9235.872.85
270892-7089234.79635.25
372878-7287835.77136.21
473322-7332235.98936.42
568798-6879833.76834.24
674816-7481636.72237.19
60min182097-8209740.29641.591.7240.9042.231.73
285313-8531341.87442.52
384466-8446641.45942.10
486333-8633342.37543.01
584702-8470241.57542.23
685518-8551841.97542.64
90min196108-9610847.17348.783.3848.0049.653.36
295418-9541846.83447.71
399561-9956148.86849.74
498813-9881348.50149.37
5103736-10373650.91751.81
6102615-10261550.36751.27
120min1104147-10414751.11953.913.6252.2155.053.60
2111251-11125154.60655.75
3108783-10878353.39454.53
4106966-10696652.50253.64
5114869-11486956.38257.55
6112972-11297255.45056.63
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
极限1109989-10998953.98655.883.2555.3657.323.23
2114552-11455256.22657.67
3110334-11033454.15655.59
4111978-11197854.96356.39
5118673-11867358.24959.73
6117528-11752857.68759.18
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