左氨氯地平叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数20000
标示量(mg)0.8供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.101940211938641948561942421943841942730.20
216.181929261928471928860.03
单位质量响应值RSD%判断
12066.6511921.260.86数据可信
供试品溶液-24081901批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min123578-2357820.17020.723.6820.1720.723.68
225140-2514021.50621.51
323353-2335319.97819.98
424823-2482321.23521.24
10min123605-2360520.19321.935.9420.4222.165.89
227202-2720223.27023.51
326216-2621622.42722.65
425498-2549821.81322.05
15min133746-3374628.86828.553.9429.3229.033.85
232718-3271827.98928.49
335027-3502729.96430.44
432005-3200527.37927.86
20min144002-4400237.64238.343.2938.4139.133.22
245264-4526438.72239.53
343342-4334237.07737.88
446676-4667639.93040.71
30min143944-4394437.59239.954.9138.7841.174.81
248642-4864241.61142.85
348538-4853841.52242.74
445693-4569339.08940.31
45min158007-5800749.62348.522.6651.2350.182.52
255556-5555647.52649.23
358033-5803349.64551.32
455291-5529147.29948.96
60min156692-5669248.49848.151.1150.6550.361.02
256492-5649248.32750.56
355364-5536447.36249.59
456615-5661548.43250.62
90min156406-5640648.25350.364.7450.9553.094.54
259122-5912250.57753.34
362682-6268253.62256.38
457252-5725248.97751.70
极限170235-7023560.08359.951.0363.3163.241.02
270315-7031560.15263.48
370712-7071260.49163.84
469052-6905259.07162.34
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