诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.813898268389428138907953889186388720838919480.12
29.823898351389783738980940.01
单位质量响应值RSD%判断
396732.72396954.580.04数据可信
供试品溶液-240821批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1533095-53309512.04210.5324.0512.0410.5324.04
2284315-2843156.4226.42
3613794-61379413.86513.86
4411989-4119899.3069.31
5489455-48945511.05611.06
6464824-46482410.50010.50
10min11474453-147445333.30530.5510.6733.3330.5710.68
21115283-111528325.19225.20
31419244-141924432.05832.08
41377638-137763831.11831.13
51481901-148190133.47433.49
61246911-124691128.16628.18
15min12330099-233009952.63348.608.8952.7148.678.89
21867326-186732642.18042.23
32113019-211301947.72947.81
42234837-223483750.48150.55
52354706-235470653.18953.26
62008713-200871345.37345.44
20min13031061-303106168.46663.848.1768.6363.998.17
22521290-252129056.95257.07
32641978-264197859.67859.83
42948258-294825866.59666.75
53093646-309364669.88070.04
62721905-272190561.48361.62
30min13906958-390695888.25184.475.5288.5384.725.53
23453266-345326678.00378.22
33558815-355881580.38780.64
43834254-383425486.60986.87
53983113-398311389.97290.25
63699852-369985283.57383.82
45min14355784-435578498.39097.074.7598.8197.464.76
24046915-404691591.41391.76
34041983-404198391.30191.69
44420546-442054699.852100.26
54527566-4527566102.270102.70
64390179-439017999.16699.55
60min14431966-4431966100.110100.124.12100.70100.684.12
24291956-429195696.94897.45
34146752-414675293.66894.21
44539480-4539480102.539103.11
54629086-4629086104.563105.16
64555672-4555672102.905103.45
极限14461549-4461549100.779101.023.97101.53101.743.97
24349104-434910498.23998.90
34191926-419192694.68895.39
44544477-4544477102.652103.40
54658513-4658513105.228106.00
64626566-4626566104.506105.22
诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.813902865390411839046143904253390225439036210.03
29.823904482390468839045850.01
单位质量响应值RSD%判断
397922.63397615.580.06数据可信
供试品溶液-E001批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1466539-46653910.51412.519.9410.5112.519.95
2594992-59499213.40913.41
3573210-57321012.91812.92
4509264-50926411.47711.48
5607838-60783813.69813.70
6579244-57924413.05413.05
10min11361453-136145330.68133.685.0030.7033.705.00
21577794-157779435.55735.58
31517625-151762534.20134.22
41463717-146371732.98633.01
51523634-152363434.33634.36
61523903-152390334.34234.36
15min12216113-221611349.94252.903.0350.0152.983.04
22426698-242669854.68754.77
32351208-235120852.98653.06
42339217-233921752.71652.79
52368643-236864353.37953.46
62382066-238206653.68253.76
20min12924002-292400265.89468.292.3566.0568.462.35
23132361-313236170.59070.76
32997622-299762267.55367.72
43034036-303403668.37468.54
53016719-301671967.98468.15
63076917-307691769.34069.51
30min13820373-382037386.09587.771.6486.3688.051.64
24000620-400062090.15790.45
33844331-384433186.63586.91
43923568-392356888.42088.70
53888787-388878787.63687.92
63889629-388962987.65587.94
45min14317760-431776097.30498.371.2297.7198.791.22
24452620-4452620100.343100.78
34316479-431647997.27597.70
44396563-439656399.08099.50
54338163-433816397.76398.19
64368193-436819398.44098.87
60min14403732-440373299.241100.111.4799.81100.701.47
24540115-4540115102.315102.92
34373941-437394198.57099.16
44440768-4440768100.076100.66
54395544-439554499.05799.65
64500429-4500429101.420102.01
极限14414559-441455999.485100.311.33100.22101.061.33
24539500-4539500102.301103.08
34392285-439228598.98399.73
44418920-441892099.583100.34
54432669-443266999.893100.65
64508533-4508533101.603102.37
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