依折麦布片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号ZT-705-231101-1-D对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.153444973448753447993450433450123448450.07
210.113483163484133483640.02
单位质量响应值RSD%判断
33974.8834457.371.00数据可信
供试品溶液-2024012321批-pH4.5(内含%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1129764-12976437.92741.9015.8437.9341.9015.85
2184374-18437453.88853.89
3123382-12338236.06136.06
4151147-15114744.17644.18
5143923-14392342.06542.07
6127526-12752637.27337.27
10min1264922-26492277.43078.617.4277.5478.747.43
2294966-29496686.21186.37
3261850-26185076.53276.64
4291450-29145085.18385.32
5245505-24550571.75571.88
6255136-25513674.57074.68
15min1309403-30940390.43191.433.1690.7891.803.18
2325715-32571595.19895.62
3312799-31279991.42391.76
4320573-32057393.69594.08
5297087-29708786.83187.17
6311425-31142591.02291.36
20min1326824-32682495.52295.431.4596.1496.061.48
2333584-33358497.49898.20
3325663-32566395.18395.80
4329058-32905896.17596.84
5319531-31953193.39193.99
6324329-32432994.79395.40
30min1331792-33179296.97496.860.7797.8897.780.80
2335066-33506697.93198.93
3330115-33011596.48497.38
4332527-33252797.18998.15
5331400-33140096.86097.74
6327477-32747795.71396.61
45min1332625-33262597.21897.330.6198.4198.550.62
2334976-33497697.90599.20
3333766-33376697.55198.74
4333657-33365797.51998.77
5333868-33386897.58198.75
6329234-32923496.22797.41
60min1333143-33314397.36997.500.9398.8699.000.93
2334679-33467997.81899.40
3334180-33418097.67299.15
4333873-33387397.58399.12
5337537-33753798.653100.12
6328079-32807995.88997.36
极限1333580-33358097.49797.840.7899.2899.640.76
2335066-33506697.93199.81
3338178-33817898.841100.61
4333110-33311097.36099.19
5337209-33720998.558100.32
6331381-33138196.85498.61
依折麦布片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号ZT-705-231101-1-D对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.153479943476643482063490303482463482280.15
210.113448563471153459860.47
单位质量响应值RSD%判断
34308.1834222.160.18数据可信
供试品溶液-2024012321批-sds1
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1214734-21473462.66846.7628.7762.6746.7628.77
2125921-12592136.74936.75
3171059-17105949.92249.92
4100896-10089629.44629.45
5139443-13944340.69540.70
6209254-20925461.06961.07
10min1298639-29863987.15580.718.9087.3480.858.93
2273916-27391679.94080.05
3282487-28248782.44282.59
4257548-25754875.16375.25
5240840-24084070.28770.41
6305918-30591889.28089.46
15min1311508-31150890.91190.802.5991.3691.182.62
2311546-31154690.92291.27
3308917-30891790.15590.55
4312493-31249391.19991.51
5298591-29859187.14187.47
6323778-32377894.49294.94
20min1313634-31363491.53293.411.8692.2594.061.84
2316576-31657692.39093.01
3314670-31467091.83492.50
4324851-32485194.80595.39
5322672-32267294.16994.76
6328028-32802895.73296.47
30min1314453-31445391.77194.632.7892.7795.572.73
2317792-31779292.74593.65
3316232-31623292.29093.23
4333760-33376097.40598.28
5331020-33102096.60697.48
6332338-33233896.99098.01
45min1314477-31447791.77894.912.9293.0596.132.88
2318809-31880993.04294.22
3316784-31678492.45193.67
4334889-33488997.73598.90
5331996-33199696.89098.06
6334322-33432297.56998.88
60min1313118-31311891.38194.643.0892.9396.143.03
2317080-31708092.53793.99
3315730-31573092.14393.64
4335307-33530797.85799.31
5331599-33159996.77598.23
6332844-33284497.13898.74
极限1331001-33100196.60098.912.7698.42100.702.70
2340542-34054299.384101.12
3356468-356468104.032105.81
4337846-33784698.598100.35
5331688-33168896.80098.55
6335988-33598898.05599.95
依折麦布片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号ZT-705-231101-1-D对照品来源中检院对照品使用方法直接使用
对照品含量(%)100对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.153481673484493483463486813488273484940.08
210.113459933483523471720.49
单位质量响应值RSD%判断
34334.3834339.470.02数据可信
供试品溶液-2024012321批-sds2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1137347-13734740.00038.0012.5440.0038.0012.54
2140004-14000440.77440.77
3132550-13255038.60338.60
4141041-14104141.07641.08
597772-9777228.47428.47
6134132-13413239.06339.06
10min1237927-23792769.29272.136.6869.4172.256.69
2258203-25820375.19775.32
3249842-24984272.76272.88
4272688-27268879.41579.54
5225302-22530265.61565.70
6242145-24214570.52070.64
15min1284091-28409182.73686.274.4683.0686.604.47
2306242-30624289.18789.54
3297910-29791086.76187.09
4314705-31470591.65292.01
5279565-27956581.41881.70
6294786-29478685.85186.18
20min1310906-31090690.54691.921.9691.1292.511.98
2320583-32058393.36493.98
3313567-31356791.32191.92
4325709-32570994.85795.49
5310382-31038290.39390.92
6312563-31256391.02891.61
30min1328562-32856295.68895.221.2296.5496.081.23
2328505-32850595.67196.57
3321037-32103793.49694.36
4332156-33215696.73497.66
5327871-32787195.48696.28
6323588-32358894.23995.10
45min1331486-33148696.53996.031.1997.6797.181.19
2330607-33060796.28397.47
3324043-32404394.37295.52
4334926-33492697.54198.75
5331144-33114496.44097.52
6326306-32630695.03196.17
60min1331247-33124796.47096.061.1097.8997.501.10
2330886-33088696.36497.84
3324690-32469094.56095.99
4334256-33425697.34698.85
5331674-33167496.59497.97
6326273-32627395.02196.45
极限1332664-33266496.88297.160.9298.6098.880.91
2332818-33281896.92798.69
3338307-33830798.526100.24
4334966-33496697.55399.35
5333898-33389897.24298.90
6328967-32896795.80697.52
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