叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数25000
标示量(mg)0.4供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.11 9703796940969809686597006969660.07
210.149552595491955080.03
单位质量响应值RSD%判断
9591.109418.931.29数据可信
供试品溶液-第1批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min19690-969016.73716.7516.7916.7416.7516.80
29101-910115.72015.72
312361-1236121.35021.35
47610-761013.14413.14
58866-886615.31415.31
610564-1056418.24618.25
10min124953-2495343.10042.7710.9343.2942.9610.91
229366-2936650.72250.90
326160-2616045.18445.42
422958-2295839.65439.80
522017-2201738.02838.20
623133-2313339.95640.16
15min134027-3402758.77255.454.0559.4456.114.04
231312-3131254.08354.82
333086-3308657.14757.89
430995-3099553.53554.12
532443-3244356.03756.63
630764-3076453.13653.78
20min136188-3618862.50563.615.1563.8264.895.13
237491-3749164.75666.09
339256-3925667.80469.18
435216-3521660.82662.01
534376-3437659.37560.59
638450-3845066.41267.65
30min142570-4257073.52874.941.9575.5476.921.99
243941-4394175.89677.95
344687-4468777.18579.31
442539-4253973.47575.33
543575-4357575.26477.14
643013-4301374.29376.27
45min149127-4912784.85481.282.9087.6884.102.81
245012-4501277.74680.65
347703-4770382.39485.38
446837-4683780.89883.57
546500-4650080.31683.03
647162-4716281.46084.26
60min145109-4510977.91481.778.0181.6985.497.72
249483-4948385.46989.23
349761-4976185.94989.85
449187-4918784.95788.53
540548-4054870.03673.64
649954-4995486.28289.99
90min145457-4545778.51583.464.3883.1588.094.11
247147-4714781.43486.15
348071-4807183.03087.89
451518-5151888.98393.50
547912-4791282.75587.14
649827-4982786.06390.73
极限152474-5247490.63587.811.8296.1493.361.66
250810-5081087.76193.38
349658-4965885.77191.55
450886-5088687.89293.40
550428-5042887.10192.40
650767-5076787.68693.31
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数25000
标示量(mg)0.4供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.11 9470594807946349485294634947260.11
210.149363493428935310.16
单位质量响应值RSD%判断
9369.549223.961.11数据可信
供试品溶液-第2批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min110758-1075818.99723.039.3119.0023.039.31
212685-1268522.40022.40
313698-1369824.18924.19
413274-1327423.44023.44
513861-1386124.47724.48
613970-1397024.66924.67
10min123904-2390442.21244.283.6942.4244.543.70
224406-2440643.09843.35
325520-2552045.06545.33
425623-2562345.24745.51
524619-2461943.47443.75
626394-2639446.60946.88
15min131354-3135455.36858.302.9756.0559.052.99
233406-3340658.99159.72
333747-3374759.59360.36
432810-3281057.93958.70
532669-3266957.69058.44
634101-3410160.21961.01
20min138621-3862168.20066.904.5669.5068.294.48
237332-3733265.92467.31
338764-3876468.45369.88
437464-3746466.15767.56
535021-3502161.84363.24
640095-4009570.80372.26
30min144989-4498979.44576.544.0481.5078.683.97
240862-4086272.15874.27
344409-4440978.42180.61
442820-4282075.61577.76
541912-4191274.01276.09
645074-4507479.59681.84
45min147952-4795284.67884.595.0387.6187.584.92
248861-4886186.28389.20
350827-5082789.75592.82
445310-4531080.01282.99
544795-4479579.10382.01
649655-4965587.68590.82
60min151500-5150090.94388.093.8794.8292.023.81
250007-5000788.30792.18
351158-5115890.33994.40
448227-4822785.16389.03
546899-4689982.81886.60
651530-5153090.99695.10
90min152556-5255692.80891.154.1097.7096.064.04
251549-5154991.03095.89
354310-5431095.905100.97
449791-4979187.92592.74
548584-4858485.79490.50
652927-5292793.46398.58
极限154167-5416795.65393.232.19101.5799.152.19
252597-5259792.88098.75
354120-5412095.570101.70
451654-5165491.21597.01
551504-5150490.95096.61
652718-5271893.09499.25
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