叶酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)92对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.411591718159205415926651591382159129615918230.04
210.361584182158424115842120.01
单位质量响应值RSD%判断
152912.87152916.220.01数据可信
供试品溶液-23041101批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11800227-180022797.47898.371.9197.4898.371.90
21767905-176790595.72895.73
31873419-1873419101.442101.44
41826010-182601098.87598.87
51815610-181561098.31198.31
61817142-181714298.39498.39
10min11809958-180995898.00598.912.1498.1799.072.13
21766579-176657995.65795.82
31883565-1883565101.991102.16
41847820-1847820100.056100.22
51825803-182580398.86399.03
61825864-182586498.86799.03
15min11809047-180904797.95698.772.0498.2899.102.04
21768706-176870695.77296.09
31879915-1879915101.793102.13
41844948-184494899.900100.23
51821358-182135898.62398.95
61821024-182102498.60598.93
20min11804177-180417797.69298.562.1298.1899.052.12
21761263-176126395.36995.85
31876955-1876955101.633102.14
41841934-184193499.737100.23
51819215-181921598.50799.00
61817786-181778698.42998.92
30min11800355-180035597.48598.422.1398.1499.082.13
21759013-175901395.24795.88
31875101-1875101101.533102.21
41838242-183824299.537100.20
51816704-181670498.37199.03
61816191-181619198.34399.00
45min11796899-179689997.29898.262.1598.1199.082.15
21755358-175535895.04995.85
31872178-1872178101.374102.22
41835358-183535899.381100.21
51815822-181582298.32399.14
61812733-181273398.15698.98
极限11793877-179387797.13598.082.2198.1199.062.21
21751464-175146494.83895.79
31873060-1873060101.422102.44
41827704-182770498.96699.96
51811679-181167998.09999.08
61809897-180989798.00298.99
叶酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)92对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.411585758158488415851711584431158445115849390.04
210.361579850157824315790460.08
单位质量响应值RSD%判断
152251.59152417.570.08数据可信
供试品溶液-23050401批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11784188-178418896.97892.069.5996.9892.069.59
21878544-1878544102.106102.11
31675986-167598691.09791.10
41657317-165731790.08290.08
51405297-140529776.38476.38
61760824-176082495.70895.71
10min11861456-1861456101.178100.944.74101.34101.104.75
21953859-1953859106.200106.37
31901039-1901039103.329103.48
41849476-1849476100.527100.68
51693891-169389192.07092.20
61883139-1883139102.356102.52
15min11859975-1859975101.097102.851.93101.43103.171.94
21955007-1955007106.263106.61
31907392-1907392103.674104.00
41855077-1855077100.831101.15
51891711-1891711102.822103.10
61883976-1883976102.402102.73
20min11854880-1854880100.820102.651.94101.32103.141.94
21948791-1948791105.925106.45
31905050-1905050103.547104.04
41850081-1850081100.559101.05
51894913-1894913102.996103.45
61877344-1877344102.041102.54
30min11851917-1851917100.659102.451.92101.33103.121.92
21945063-1945063105.722106.42
31900095-1900095103.278103.95
41846843-1846843100.383101.04
51891112-1891112102.790103.41
61874578-1874578101.891102.56
45min11845308-1845308100.300102.181.93101.13103.021.93
21939566-1939566105.423106.30
31895093-1895093103.006103.85
41842379-1842379100.141100.96
51886956-1886956102.564103.36
61870415-1870415101.665102.51
极限11844684-1844684100.266101.991.90101.27103.001.90
21935116-1935116105.181106.23
31892015-1892015102.839103.85
41838312-183831299.920100.91
51882989-1882989102.348103.31
61865403-1865403101.392102.40
叶酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)92对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.411581016158099315802631581987158130515811130.04
210.361582232158154715818900.04
单位质量响应值RSD%判断
151884.05152692.080.38数据可信
供试品溶液-23050402批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11932475-1932475105.071102.332.20105.07102.332.20
21859437-1859437101.099101.10
31856013-1856013100.913100.91
41859681-1859681101.113101.11
51847281-1847281100.439100.44
61937527-1937527105.345105.35
10min11934653-1934653105.189102.782.11105.36102.952.11
21875358-1875358101.965102.13
31860746-1860746101.171101.34
41872286-1872286101.798101.97
51852600-1852600100.728100.90
61946186-1946186105.816105.99
15min11931192-1931192105.001102.572.09105.35102.912.09
21872614-1872614101.816102.15
31856732-1856732100.952101.29
41867945-1867945101.562101.90
51849335-1849335100.550100.89
61940881-1940881105.528105.88
20min11932448-1932448105.069102.702.13105.59103.212.12
21875422-1875422101.969102.48
31858346-1858346101.040101.55
41869524-1869524101.648102.16
51851231-1851231100.653101.16
61945752-1945752105.793106.32
30min11929953-1929953104.934102.532.18105.63103.212.18
21871847-1871847101.774102.45
31854691-1854691100.841101.51
41865872-1865872101.449102.13
51847329-1847329100.441101.11
61944601-1944601105.730106.43
45min11923388-1923388104.577102.272.09105.45103.122.09
21867753-1867753101.552102.40
31850178-1850178100.596101.44
41863015-1863015101.294102.14
51844705-1844705100.298101.14
61936727-1936727105.302106.18
极限11922474-1922474104.527102.052.23105.58103.082.23
21862145-1862145101.247102.26
31844635-1844635100.295101.30
41856811-1856811100.957101.97
51839371-1839371100.008101.01
61936342-1936342105.281106.34
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