盐酸司来吉兰片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号101298-201801对照品来源中检院对照品使用方法减压干燥3h
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数1000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.912409952411172409522408712407212409310.07
29.992383862400222392040.49
单位质量响应值RSD%判断
24311.9123944.341.08数据可信
供试品溶液-2095120批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min194089-9408969.84576.537.6169.8576.537.60
2109979-10997981.64181.64
3114831-11483185.24385.24
4101895-10189575.64075.64
597503-9750372.37972.38
6100236-10023674.40874.41
10min1112440-11244083.46889.325.2283.5889.455.22
2124032-12403292.07392.21
3130187-13018796.64296.78
4119385-11938588.62388.75
5115548-11554885.77585.90
6120342-12034289.33489.46
15min1118081-11808187.65592.014.1587.9192.294.16
2127065-12706594.32494.61
3132125-13212598.08098.38
4123474-12347491.65891.93
5119383-11938388.62288.89
6123596-12359691.74992.02
20min1120075-12007589.13593.313.6389.5493.743.64
2128312-12831295.25095.70
3132762-13276298.55399.02
4125885-12588593.44893.87
5121788-12178890.40790.82
6125353-12535393.05393.48
30min1120277-12027789.28593.113.2489.8493.703.24
2127099-12709994.34994.95
3131319-13131997.48298.11
4127222-12722294.44195.02
5121590-12159090.26090.82
6125087-12508792.85693.44
45min1121956-12195690.53294.072.9591.2394.812.96
2128732-12873295.56296.32
3131554-13155497.65798.45
4129172-12917295.88896.63
5123151-12315191.41992.13
6125789-12578993.37794.11
60min1123262-12326291.50194.892.9092.3595.792.91
2129120-12912095.85096.77
3132827-13282798.60299.56
4130619-13061996.96297.86
5124307-12430792.27793.14
6126862-12686294.17495.06
极限1124884-12488492.70595.522.7693.7196.572.76
2130309-13030996.73297.81
3132076-13207698.04499.16
4132546-13254698.39399.45
5124372-12437292.32593.34
6127872-12787294.92395.97
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