叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.111227881122723812270351226837122708612272150.04
210.141226558122490112257300.10
单位质量响应值RSD%判断
121386.25120880.670.30数据可信
供试品溶液-24092402批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1134157-13415718.18117.806.0318.1817.806.03
2134488-13448818.22618.23
3135879-13587918.41418.41
4115569-11556915.66215.66
5136382-13638218.48318.48
6131686-13168617.84617.85
10min1234000-23400031.71231.534.3131.9131.734.33
2237624-23762432.20332.41
3241855-24185532.77632.98
4213162-21316228.88829.06
5235858-23585831.96432.17
6233656-23365631.66531.86
15min1310645-31064542.09941.853.8842.6542.403.90
2313903-31390342.54043.10
3318565-31856543.17243.74
4285004-28500438.62439.12
5313152-31315242.43943.00
6311588-31158842.22742.78
20min1369015-36901550.00949.733.5751.0350.743.58
2383651-38365151.99353.03
3372400-37240050.46851.52
4343690-34369046.57747.50
5365988-36598849.59950.63
6366967-36696749.73250.75
30min1438130-43813059.37659.102.3460.9560.672.38
2438649-43864959.44661.06
3445675-44567560.39862.01
4416147-41614756.39657.84
5439813-43981359.60461.19
6438262-43826259.39460.97
45min1503626-50362668.25268.422.0370.4970.642.06
2503756-50375668.26970.54
3518294-51829470.23972.52
4487998-48799866.13468.20
5512104-51210469.40171.65
6503560-50356068.24370.47
60min1548379-54837974.31773.791.7477.3176.771.76
2534785-53478572.47475.50
3552207-55220774.83577.90
4531008-53100871.96274.77
5554175-55417575.10278.12
6546419-54641974.05177.04
90min1589553-58955379.89779.681.1083.7283.481.15
2581780-58178078.84382.68
3595053-59505380.64284.53
4578999-57899978.46682.07
5594073-59407380.50984.36
6588081-58808179.69783.51
极限1605270-60527082.02782.620.8386.7487.310.88
2611974-61197482.93587.65
3613635-61363583.16087.95
4603490-60349081.78586.26
5616138-61613883.49988.24
6607356-60735682.30987.01
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.111225497122358712236761222621122269612236150.10
210.141221195121974712204710.09
单位质量响应值RSD%判断
121030.17120362.030.40数据可信
供试品溶液-24092403批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1133591-13359118.17018.012.1318.1718.012.14
2133929-13392918.21618.22
3127368-12736817.32417.32
4131069-13106917.82717.83
5133502-13350218.15818.16
6135146-13514618.38118.38
10min1239485-23948532.57332.361.7232.7732.561.73
2240300-24030032.68432.89
3232987-23298731.68931.88
4233842-23384231.80532.00
5243765-24376533.15533.36
6237271-23727132.27232.48
15min1317595-31759543.19742.891.2743.7643.451.28
2314286-31428642.74743.31
3311565-31156542.37742.92
4310717-31071742.26142.81
5321363-32136343.70944.28
6316649-31664943.06843.63
20min1372816-37281650.70750.141.7151.7551.181.70
2366363-36636349.83050.87
3363023-36302349.37650.39
4360283-36028349.00350.02
5375142-37514251.02452.08
6374193-37419350.89551.94
30min1446019-44601960.66459.331.4862.2760.931.48
2433941-43394159.02160.62
3429543-42954358.42359.99
4430376-43037658.53660.10
5441510-44151060.05161.67
6436009-43600959.30260.91
45min1504664-50466468.64067.661.1070.9269.921.09
2493237-49323767.08669.34
3495334-49533467.37169.58
4492274-49227466.95569.17
5495369-49536967.37669.67
6503924-50392468.54070.81
60min1545763-54576374.23072.901.3777.2775.911.36
2539451-53945173.37276.37
3528821-52882171.92674.89
4526827-52682771.65574.61
5534427-53442772.68975.73
6540693-54069373.54176.57
90min1592079-59207980.53078.811.4884.4082.631.46
2579989-57998978.88682.70
3573853-57385378.05181.81
4568885-56888577.37581.13
5575550-57555078.28282.13
6586377-58637779.75483.60
极限1605836-60583682.40181.591.4687.1686.281.43
2600756-60075681.71086.40
3590826-59082680.35984.99
4593840-59384080.76985.39
5594129-59412980.80985.52
6613707-61370783.47288.20
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