叶酸项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数25000
标示量(mg)0.4供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.119889998599986389857298531986480.15
210.149713196689969100.33
单位质量响应值RSD%判断
9757.479557.201.47数据可信
供试品溶液-24092404批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min124629-2462941.87049.639.9441.8749.639.94
227310-2731046.42846.43
332788-3278855.74155.74
431283-3128353.18253.18
529389-2938949.96249.96
629770-2977050.61050.61
10min144581-4458175.78966.926.9776.2567.466.86
236655-3665562.31562.83
338508-3850865.46566.08
438836-3883666.02266.61
539604-3960467.32867.88
637983-3798364.57265.13
15min145617-4561777.55076.081.3378.8677.371.32
244462-4446275.58776.80
344505-4450575.66077.01
445305-4530577.02078.34
544574-4457475.77777.08
644032-4403274.85676.14
20min149341-4934183.88181.941.6886.0584.081.69
247503-4750380.75782.80
348050-4805081.68683.87
449030-4903083.35385.53
547892-4789281.41883.56
647375-4737580.53982.65
30min153827-5382791.50889.641.5794.6192.701.56
252259-5225988.84291.79
352209-5220988.75791.85
453667-5366791.23694.34
551816-5181688.08991.14
652609-5260989.43792.44
45min156507-5650796.06494.061.93100.1898.111.88
255566-5556694.46498.40
355339-5533994.07898.16
455905-5590595.04099.16
553355-5335590.70594.73
655297-5529794.00798.01
60min157096-5709697.06597.040.90102.25102.140.82
258060-5806098.704103.69
356928-5692896.779101.91
456826-5682696.606101.78
557022-5702296.939101.98
656566-5656696.164101.21
90min157902-5790298.43597.401.33104.70103.571.26
257941-5794198.501104.58
357355-5735597.505103.71
456914-5691496.756103.01
555960-5596095.134101.25
657694-5769498.082104.19
极限157818-5781898.29297.251.19105.65104.501.13
257473-5747397.706104.88
357565-5756597.862105.15
456404-5640495.889103.21
556282-5628295.681102.85
657679-5767998.056105.26
叶酸项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数25000
标示量(mg)0.4供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.119613695815957119575295648958120.20
210.149453193997942640.41
单位质量响应值RSD%判断
9476.959296.251.37数据可信
供试品溶液-24092405批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min122033-2203338.53742.3517.6638.5442.3517.66
221877-2187738.26438.26
322989-2298940.20940.21
423600-2360041.27741.28
532821-3282157.40557.41
621943-2194338.37938.38
10min133450-3345058.50560.873.5558.9361.343.62
233462-3346258.52658.95
335937-3593762.85563.30
435241-3524161.63862.10
536328-3632863.53964.18
634380-3438060.13260.56
15min140465-4046570.77573.262.9971.8574.413.03
240379-4037970.62471.70
343322-4332275.77276.92
442768-4276874.80375.95
542691-4269174.66876.01
641695-4169572.92674.02
20min144254-4425477.40280.132.8179.2782.102.85
244365-4436577.59679.46
346873-4687381.98383.97
446939-4693982.09884.07
546933-4693382.08884.26
645528-4552879.63081.54
30min149090-4909085.86088.773.1488.5891.623.17
248495-4849584.82087.54
351758-5175890.52793.42
452108-5210891.13994.03
552123-5212391.16594.25
650933-5093389.08491.87
45min152631-5263192.05495.332.8695.7399.172.90
252614-5261492.02495.69
354975-5497596.153100.06
456046-5604698.027101.93
556054-5605498.041102.14
654702-5470295.67699.46
60min154573-5457395.45099.233.91100.15104.133.91
254447-5444795.23099.92
356830-5683099.398104.37
457173-5717399.998104.99
560539-60539105.885111.07
656856-5685699.443104.29
90min157145-5714599.949101.511.60105.71107.511.72
256753-5675399.263105.01
358651-58651102.583108.66
458740-58740102.738108.84
559015-59015103.219109.58
657939-57939101.337107.28
极限158458-58458102.245102.020.67109.12109.150.81
257801-57801101.096107.94
358567-58567102.436109.65
458395-58395102.135109.38
558819-58819102.877110.39
657947-57947101.351108.42
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