叶酸左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105 对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数5000
标示量(mg)2.5供试品稀释倍数2系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.26 7668276583764957628576212764510.26
217.217477675156749660.36
单位质量响应值RSD%判断
4429.374355.961.19数据可信
供试品溶液-8153342批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min160096-60096138.216136.623.58138.22136.623.58
258543-58543134.644134.64
362401-62401143.517143.52
460490-60490139.122139.12
556124-56124129.081129.08
658746-58746135.111135.11
10min171443-71443164.313162.436.76165.85163.956.71
261014-61014140.327141.82
372804-72804167.443169.04
473680-73680169.458171.00
572883-72883167.625169.06
671923-71923165.417166.92
15min176428-76428175.778176.512.82179.14179.832.81
274705-74705171.816174.87
375759-75759174.240177.69
480676-80676185.548188.98
575358-75358173.317176.61
677552-77552178.363181.70
20min181125-81125186.581181.712.11191.90187.002.11
277194-77194177.540182.50
378619-78619180.817186.21
478925-78925181.521187.01
577371-77371177.947183.17
680816-80816185.870191.19
30min183526-83526192.103190.222.99199.49197.522.93
279918-79918183.805190.74
379231-79231182.225189.63
484256-84256193.782201.29
584527-84527194.405201.61
684774-84774194.973202.36
45min183392-83392191.795188.981.94201.32198.401.91
279693-79693183.288192.27
383659-83659192.409201.83
480734-80734185.682195.34
582916-82916190.700200.06
682620-82620190.019199.57
60min183954-83954193.088191.431.53204.74202.951.52
281278-81278186.933197.95
384362-84362194.026205.59
482125-82125188.881200.60
584339-84339193.973205.45
683343-83343191.682203.35
90min1-0.0000.00-13.8013.642.05
2-0.00013.09
3-0.00013.72
4-0.00013.82
5-0.00013.63
6-0.00013.79
极限1-0.0000.00-13.8013.642.05
2-0.00013.09
3-0.00013.72
4-0.00013.82
5-0.00013.63
6-0.00013.79
叶酸左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105 对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数5000
标示量(mg)2.5供试品稀释倍数2系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.26 7466374071744837417373888742560.43
217.217363773672736540.04
单位质量响应值RSD%判断
4302.204279.720.38数据可信
供试品溶液-8153342批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min142538-42538100.14797.352.93100.1597.352.93
241898-4189898.64098.64
341200-4120096.99797.00
439145-3914592.15892.16
541147-4114796.87296.87
642178-4217899.29999.30
10min143078-43078101.41899.151.99102.53100.231.99
242147-4214799.226100.32
341018-4101896.56897.65
441191-4119196.97598.00
542625-42625100.351101.43
642617-42617100.333101.44
15min144187-44187104.02997.893.64106.27100.083.60
240423-4042395.16797.37
340827-4082796.11898.27
440061-4006194.31596.42
541825-4182598.468100.66
642166-4216699.271101.49
20min141420-4142097.51497.082.01100.91100.362.00
240750-4075095.93799.19
340085-4008594.37297.59
440859-4085996.19499.34
542132-4213299.191102.48
642179-4217999.301102.62
30min141682-4168298.13195.922.57102.61100.272.55
240756-4075695.951100.27
340307-4030794.89499.16
438899-3889991.57995.80
541641-4164198.035102.42
641178-4117896.945101.37
45min141058-4105896.66294.273.12102.2399.683.06
239253-3925392.41397.80
338553-3855390.76596.09
438976-3897691.76197.00
541013-4101396.556102.03
641398-4139897.463102.96
60min140402-4040295.11893.291.51101.7699.761.55
239133-3913392.13098.55
339472-3947292.92899.26
438838-3883891.43697.69
539770-3977093.630100.18
640141-4014194.503101.09
90min139574-3957493.16892.121.80100.8799.621.81
238499-3849990.63898.08
338695-3869591.09998.46
438414-3841490.43797.71
539423-3942392.813100.40
640170-4017094.572102.21
极限139420-3942092.80691.172.27101.5499.692.24
238725-3872591.17099.62
338572-3857290.80999.18
437082-3708287.30295.58
539402-3940292.764101.38
639140-3914092.147100.83
叶酸左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105 对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数5000
标示量(mg)2.5供试品稀释倍数2系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.26 7482774558746847518175018748540.34
217.217424074429743340.18
单位质量响应值RSD%判断
4336.854319.230.29数据可信
供试品溶液-8153342批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min140957-4095795.59898.243.7595.6098.243.75
241216-4121696.20396.20
342876-42876100.077100.08
440332-4033294.13994.14
542525-4252599.25899.26
644637-44637104.188104.19
10min144944-44944104.904101.152.14105.97102.242.11
242228-4222898.56599.63
342795-4279599.888101.00
443230-43230100.904101.95
543669-43669101.928103.03
643143-43143100.700101.86
15min141729-4172997.40099.164.4199.63101.384.34
240008-4000893.38395.55
344846-44846104.675106.90
441209-4120996.18698.35
544367-44367103.557105.79
642738-4273899.755102.03
20min142123-4212398.320100.062.68101.63103.382.66
240944-4094495.56898.77
343533-43533101.611105.00
443002-43002100.371103.61
544033-44033102.778106.16
643589-43589101.741105.13
30min141996-4199698.02397.683.21102.43102.113.17
239641-3964192.52696.79
341950-4195097.916102.43
441194-4119496.151100.50
543480-43480101.487106.02
642838-4283899.989104.50
45min141739-4173997.42397.353.30102.91102.863.25
239792-3979292.87998.17
343387-43387101.270106.87
440565-4056594.683100.10
541770-4177097.496103.15
642998-42998100.362105.99
60min140814-4081495.26496.462.41101.84103.062.39
240298-4029894.060100.38
342628-4262899.498106.23
440863-4086395.379101.85
542539-4253999.291106.03
640819-4081995.276102.02
90min141128-4112895.99795.371.83103.63103.031.81
240573-4057394.702102.07
340668-4066894.924102.76
439694-3969492.650100.18
541922-4192297.851105.69
641159-4115996.070103.87
极限140185-4018593.79695.622.04102.50104.352.04
240190-4019093.808102.23
341185-4118596.130105.02
440411-4041194.324102.88
541671-4167197.265106.19
642157-4215798.399107.27
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