氨氯地平阿托伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100374-202106 对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
115.399678996495966809653396679966350.13
215.459768897638976630.04
单位质量响应值RSD%判断
6279.086321.230.48数据可信
供试品溶液-LA6362批-氨氯地平-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min160390-6039062.13960.863.1362.1460.863.14
259806-5980661.53861.54
356761-5676158.40558.40
458677-5867760.37660.38
557518-5751859.18459.18
661710-6171063.49763.50
10min178162-7816280.42580.462.5680.5380.562.56
278180-7818080.44480.55
374780-7478076.94577.04
480366-8036682.69382.79
580018-8001882.33582.43
677673-7767379.92280.03
15min181648-8164884.01285.723.6584.2585.963.64
283317-8331785.73085.97
378400-7840080.67080.90
487232-8723289.75890.00
585041-8504187.50387.74
684198-8419886.63686.88
20min183823-8382386.25088.113.7186.6388.493.70
285787-8578788.27188.65
380732-8073283.07083.43
489808-8980892.40992.80
587975-8797590.52290.90
685659-8565988.13988.52
30min184995-8499587.45688.533.5387.9889.063.53
285972-8597288.46188.99
381351-8135183.70784.21
488822-8882291.39491.94
589860-8986092.46292.99
685218-8521887.68688.22
45min185071-8507187.53488.542.6888.2089.212.69
285312-8531287.78288.46
382498-8249884.88785.52
488781-8878191.35292.05
588255-8825590.81191.50
686351-8635188.85189.53
极限185660-8566088.14088.723.0288.9589.543.02
284915-8491587.37488.19
382605-8260584.99785.78
486957-8695789.47590.32
590458-9045893.07793.92
686728-8672889.23990.06
氨氯地平阿托伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100590-202005 对照品来源中检院对照品使用方法直接使用
对照品含量(%)94.9对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数0.9671
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.333558043553613553043566173572553560680.24
211.303589123591073590100.04
单位质量响应值RSD%判断
31427.0131770.800.77数据可信
供试品溶液-LA6362批-阿托伐他汀钙-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1212764-21276455.61854.252.8955.6254.252.89
2209328-20932854.72054.72
3198823-19882351.97451.97
4203990-20399053.32553.32
5205268-20526853.65953.66
6214968-21496856.19556.19
10min1285851-28585174.72475.353.1074.8275.443.10
2291549-29154976.21476.30
3272057-27205771.11871.20
4297198-29719877.69077.78
5294497-29449776.98477.07
6288225-28822575.34575.44
15min1306156-30615680.03281.023.7380.2581.243.72
2309376-30937680.87481.09
3291695-29169576.25276.46
4324643-32464384.86585.08
5319903-31990383.62683.84
6307898-30789880.48780.71
20min1312331-31233181.64682.854.0382.0083.214.02
2315581-31558182.49682.85
3297570-29757077.78878.12
4333903-33390387.28587.65
5327917-32791785.72186.08
6314422-31442282.19382.55
30min1317380-31738082.96684.024.0683.4584.514.06
2320918-32091883.89184.38
3302074-30207478.96579.43
4338884-33888488.58789.09
5332838-33283887.00787.51
6316491-31649182.73483.22
45min1316386-31638682.70683.924.0783.3384.554.06
2321238-32123883.97584.60
3301767-30176778.88579.48
4338425-33842588.46789.12
5332428-33242886.90087.54
6315999-31599982.60583.23
极限1317780-31778083.07184.163.8583.8384.933.85
2321163-32116383.95584.73
3303275-30327579.27980.00
4337712-33771288.28189.08
5333637-33363787.21688.01
6318186-31818683.17783.94
氨氯地平阿托伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100374-202106 对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
115.399680797197973789676796881970060.28
215.459827198089981800.14
单位质量响应值RSD%判断
6303.186354.690.58数据可信
供试品溶液-LA6362批-氨氯地平-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min155982-5598257.34157.138.1357.3457.138.14
261778-6177863.27863.28
356707-5670758.08458.08
453268-5326854.56154.56
558394-5839459.81259.81
648516-4851649.69449.69
10min172823-7282374.59180.375.1474.6980.475.14
282273-8227384.27184.38
383844-8384485.88085.98
477296-7729679.17379.26
578229-7822980.12980.23
676324-7632478.17778.26
15min177324-7732479.20286.555.4479.4286.785.44
287767-8776789.89890.14
390923-9092393.13193.37
483671-8367185.70385.93
583784-8378485.81886.05
683528-8352885.55685.77
20min177731-7773179.61887.045.7379.9787.425.73
287847-8784789.98090.38
392087-9208794.32394.72
482467-8246784.46984.84
585499-8549987.57587.95
684234-8423486.27986.64
30min179660-7966081.59488.595.2282.0889.115.21
289363-8936391.53392.08
392949-9294995.20695.76
484832-8483286.89287.40
587017-8701789.13089.65
685101-8510187.16787.67
45min180005-8000581.94889.554.8682.5790.214.86
288656-8865690.80991.51
393219-9321995.48396.19
487611-8761189.73890.39
587617-8761789.74590.42
687425-8742589.54890.19
极限194050-9405096.33491.793.9297.0992.603.89
287951-8795190.08790.94
394157-9415796.44397.31
487390-8739089.51290.31
587637-8763789.76590.59
686490-8649088.59089.38
氨氯地平阿托伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100590-202005 对照品来源中检院对照品使用方法直接使用
对照品含量(%)94.9对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数0.9671
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.333562513568893586173565383568533570300.26
211.303599323594993597160.09
单位质量响应值RSD%判断
31511.9231833.270.72数据可信
供试品溶液-LA6362批-阿托伐他汀钙-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1197202-19720251.43051.137.7451.4351.137.74
2214910-21491056.04956.05
3200608-20060852.31952.32
4187238-18723848.83248.83
5205117-20511753.49553.49
6171291-17129144.67344.67
10min1262986-26298668.58774.155.5868.6774.245.57
2299079-29907978.00078.09
3305347-30534779.63579.72
4282254-28225473.61273.69
5283636-28363673.97274.06
6272704-27270471.12171.20
15min1278982-27898272.75980.756.4772.9680.966.47
2322481-32248184.10384.33
3338858-33885888.37488.59
4306137-30613779.84180.04
5306889-30688980.03780.25
6304363-30436379.37879.57
20min1285232-28523274.38982.746.4674.7183.086.45
2328928-32892885.78486.15
3347261-34726190.56690.93
4314264-31426481.96082.30
5315263-31526382.22182.57
6312496-31249681.49981.82
30min1289058-28905875.38683.796.3475.8384.276.33
2332287-33228786.66087.17
3351056-35105691.55592.07
4318317-31831783.01783.49
5318586-31858683.08783.57
6318331-31833183.02183.48
45min1289205-28920575.42583.936.3876.0084.556.38
2332055-33205586.60087.25
3352095-35209591.82692.50
4319187-31918783.24483.86
5319527-31952783.33383.95
6318865-31886583.16083.76
极限1357654-35765493.27687.065.2193.9787.825.16
2333043-33304386.85887.65
3352628-35262891.96592.79
4319271-31927183.26684.02
5320689-32068983.63684.40
6319624-31962483.35884.10
点击查看处理图标(人工保存)
　
原始图谱下载图谱(姜进硙 于 2024-09-29 17:01:07 完成)
生成报告数据部分(等待生成报告)
Current page cost:38 ms