托伐普坦片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号101242-201201对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数10000
标示量(mg)15供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.445032150118500764997349776500530.40
216.394986449913498880.07
单位质量响应值RSD%判断
3044.593043.810.02数据可信
供试品溶液-2J95SDC1批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13036-30365.9845.849.265.985.839.24
23264-32646.4336.43
32776-27765.4715.47
43285-32856.4756.47
52749-27495.4185.42
62655-26555.2335.23
10min111220-1122022.11421.542.5822.1521.572.59
210928-1092821.53921.57
311131-1113121.93921.97
410842-1084221.36921.41
511015-1101521.71021.74
610424-1042420.54520.57
15min115934-1593431.40531.082.0031.5631.232.00
215590-1559030.72730.88
316024-1602431.58331.73
416170-1617031.87032.03
515491-1549130.53230.68
615405-1540530.36330.51
20min119290-1929038.02038.525.1438.3538.845.10
219119-1911937.68338.01
319120-1912037.68538.01
421585-2158542.54342.87
519026-1902637.50037.82
619122-1912237.68938.00
30min124492-2449248.27348.281.9848.8148.821.99
224618-2461848.52149.06
324077-2407747.45547.99
425343-2534349.95050.52
524453-2445348.19648.72
623985-2398547.27447.79
45min129999-2999959.12760.103.5359.9460.913.51
230046-3004659.22060.02
330309-3030959.73860.54
432669-3266964.38965.23
530088-3008859.30260.10
629853-2985358.83959.62
60min134633-3463368.26067.911.8169.4069.051.80
234936-3493668.85869.99
334959-3495968.90370.04
434865-3486568.71869.92
533675-3367566.37267.50
633658-3365866.33967.45
90min139943-3994378.72677.731.8980.2479.241.89
239177-3917777.21678.73
339257-3925777.37478.89
440401-4040179.62981.21
539597-3959778.04479.54
638236-3823675.36276.84
120min142871-4287184.49782.931.8386.4584.881.79
242617-4261783.99785.94
342611-4261183.98585.93
441589-4158981.97084.00
541899-4189982.58184.51
640870-4087080.55382.45
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
180min145433-4543389.54787.551.3291.9789.961.29
243805-4380586.33888.75
343959-4395986.64289.05
444424-4442487.55890.04
544662-4466288.02790.41
644250-4425087.21589.56
240min147180-4718092.99089.292.8295.9192.182.76
244678-4467888.05990.95
345952-4595290.57093.46
445510-4551089.69992.67
545119-4511988.92891.80
643375-4337585.49188.32
300min144133-4413386.98586.951.8990.4290.341.86
242915-4291584.58487.96
344123-4412386.96590.36
445095-4509588.88192.35
544934-4493488.56391.93
643487-4348785.71189.02
360min145124-4512488.93888.361.2792.8692.241.24
243969-4396986.66190.51
345263-4526389.21293.09
444635-4463587.97491.94
545502-4550289.68393.54
644498-4449887.70491.49
极限145851-4585190.37189.122.3694.7993.492.23
245198-4519889.08493.42
346585-4658591.81796.19
443398-4339885.53689.99
545337-4533789.35893.72
644941-4494188.57792.85
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