左氨氯地平叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105 对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数5000
标示量(mg)2.5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.267505074689746237479774611747540.25
217.217390773913739100.01
单位质量响应值RSD%判断
4331.054294.600.60数据可信
供试品溶液-24082901批-左氨氯地平-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
10min142683-4268349.99049.661.6649.9949.661.65
242881-4288150.22250.22
343412-4341250.84450.84
442014-4201449.20649.21
541737-4173748.88248.88
641672-4167248.80648.81
15min143070-4307050.44349.172.5751.0049.722.55
242052-4205249.25149.81
341786-4178648.93949.50
442187-4218749.40949.96
542803-4280350.13050.67
640020-4002046.87147.41
20min142061-4206149.26148.261.4450.3849.361.44
240901-4090147.90349.01
341292-4129248.36149.47
440969-4096947.98249.08
541636-4163648.76449.86
640378-4037847.29048.35
30min141314-4131448.38648.322.1150.0549.962.01
240945-4094547.95449.59
340971-4097147.98549.63
441122-4112248.16249.79
540309-4030947.20948.85
642895-4289550.23851.83
45min141142-4114248.18547.301.5750.3949.471.53
239885-3988546.71348.88
340631-4063147.58749.77
440863-4086347.85850.02
540325-4032547.22849.39
639446-3944646.19948.35
60min139846-3984646.66746.291.8549.4048.991.75
240379-4037947.29149.98
339046-3904645.73048.44
438326-3832644.88747.58
539913-3991346.74649.44
639636-3963646.42149.08
90min139713-3971346.51145.831.3149.7749.041.27
239082-3908245.77248.99
339026-3902645.70748.92
439482-3948246.24149.44
539266-3926645.98849.20
638229-3822944.77347.95
极限139889-3988946.71845.681.4350.4949.401.37
238622-3862245.23448.96
338936-3893645.60149.33
439441-3944146.19349.90
538620-3862045.23148.95
638488-3848845.07748.75
左氨氯地平叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217 对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数20000
标示量(mg)0.8供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.209346994891935929319293398937080.73
216.279623895905960720.25
单位质量响应值RSD%判断
5784.445904.861.46数据可信
供试品溶液-24082901批-叶酸-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1-0.0000.00-0.000.00-
2-0.0000.00
3-0.0000.00
4-0.0000.00
5-0.0000.00
6-0.0000.00
10min113934-1393412.23211.3811.2912.2311.3811.28
214332-1433212.58112.58
311237-112379.8649.86
414141-1414112.41312.41
513027-1302711.43511.44
611091-110919.7369.74
15min123155-2315520.32618.5817.3520.4618.7117.29
224008-2400821.07521.21
314204-1420412.46912.58
423392-2339220.53420.67
522137-2213719.43219.56
620134-2013417.67417.78
20min124390-2439021.41021.224.5921.7721.554.73
225307-2530722.21522.59
322580-2258019.82120.07
424553-2455321.55321.92
525133-2513322.06222.41
623072-2307220.25320.56
30min127317-2731723.97924.063.4624.5824.633.58
228588-2858825.09525.72
326005-2600522.82823.30
427378-2737824.03324.64
528316-2831624.85625.44
626858-2685823.57624.11
45min130113-3011326.43426.373.2827.3027.213.37
231559-3155927.70328.60
329199-2919925.63126.35
429709-2970926.07926.95
530737-3073726.98227.85
628939-2893925.40326.19
60min130963-3096327.18026.545.1228.3427.675.12
232630-3263028.64329.85
329248-2924825.67426.68
429434-2943425.83827.00
530839-3083927.07128.24
628304-2830424.84625.92
90min130979-3097927.19426.066.3928.6627.496.15
232236-3223628.29729.82
330104-3010426.42627.72
429347-2934725.76127.21
526748-2674823.48024.94
628742-2874225.23026.58
极限136775-3677532.28231.562.5234.0533.272.66
236921-3692132.41034.25
334984-3498430.71032.30
436237-3623731.81033.55
536040-3604031.63733.36
634747-3474730.50232.13
左氨氯地平叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105 对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数5000
标示量(mg)2.5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.267434174742744167442874215744280.27
217.217500375435752190.41
单位质量响应值RSD%判断
4312.174370.660.96数据可信
供试品溶液-24082901批-左氨氯地平-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min141417-4141748.18947.830.7548.1947.830.75
240967-4096747.66547.67
341303-4130348.05648.06
441401-4140148.17048.17
540721-4072147.37947.38
640818-4081847.49247.49
10min142563-4256349.52249.821.7950.0650.351.78
242365-4236549.29249.82
343726-4372650.87651.41
443784-4378450.94351.48
542552-4255249.51050.04
641913-4191348.76649.29
15min142510-4251049.46149.231.8450.5550.321.80
241817-4181748.65449.73
342051-4205148.92750.03
442258-4225849.16850.27
543733-4373350.88451.96
641503-4150348.28949.36
20min140598-4059847.23648.472.9048.8750.102.83
241788-4178848.62150.24
341815-4181548.65250.29
443305-4330550.38652.03
542466-4246649.41051.05
640002-4000246.54348.15
30min139778-3977846.28248.202.3948.4450.382.27
241769-4176948.59950.76
342471-4247149.41551.60
441181-4118147.91450.12
541078-4107847.79549.99
642301-4230149.21851.34
45min141565-4156548.36147.702.5451.0450.412.39
241097-4109747.81750.51
341607-4160748.41051.14
441334-4133448.09250.83
538908-3890845.27047.99
641487-4148748.27050.94
60min138370-3837044.64446.372.6747.8649.612.53
239466-3946645.91949.15
341564-4156448.36051.63
439543-3954346.00949.28
540385-4038546.98850.21
639815-3981546.32549.53
90min139736-3973646.23347.201.4749.9450.961.41
241258-4125848.00451.74
341159-4115947.88951.70
440552-4055247.18350.97
540637-4063747.28151.03
640075-4007546.62850.35
极限138671-3867144.99445.891.6749.2250.171.60
239293-3929345.71849.99
339867-3986746.38650.73
440460-4046047.07651.39
538873-3887345.22949.50
639493-3949345.95050.19
左氨氯地平叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217 对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数20000
标示量(mg)0.8供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.209556495836955929580695771957140.14
216.279480594833948190.03
单位质量响应值RSD%判断
5908.275827.840.97数据可信
供试品溶液-24082901批-叶酸-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min114664-1466412.82014.105.5812.8214.105.58
216521-1652114.44414.44
316810-1681014.69614.70
415724-1572413.74713.75
517160-1716015.00215.00
615893-1589313.89513.89
10min120496-2049617.91918.564.0118.0618.724.02
221253-2125318.58118.74
321754-2175419.01919.18
420305-2030517.75217.90
522607-2260719.76519.93
620993-2099318.35318.51
15min123266-2326620.34120.513.9920.6820.873.98
223121-2312120.21420.58
323706-2370620.72521.10
422473-2247319.64720.00
525176-2517622.01122.40
622983-2298320.09320.45
20min125048-2504821.89921.653.8522.4722.243.83
224421-2442121.35021.94
324892-2489221.76222.37
423724-2372420.74121.31
526424-2642423.10223.73
624080-2408021.05221.63
30min127461-2746124.00823.383.8024.8224.213.77
226674-2667423.32024.15
326666-2666623.31324.16
425358-2535822.17022.97
528233-2823324.68325.57
626043-2604322.76923.58
45min129749-2974926.00925.033.7727.0926.123.73
228157-2815724.61725.70
328616-2861625.01826.12
427113-2711323.70424.75
529980-2998026.21027.37
628171-2817124.62925.70
60min131289-3128927.35525.934.0728.7227.304.00
229142-2914225.47826.84
329507-2950725.79727.18
428196-2819624.65125.96
530927-3092727.03828.49
628894-2889425.26126.60
90min133783-3378329.53527.165.3031.2128.825.14
230424-3042426.59928.24
330698-3069826.83828.51
429224-2922425.55027.13
532197-3219728.14929.90
630093-3009326.30927.93
极限142499-4249937.15537.411.6039.1539.361.67
242441-4244137.10539.04
342847-4284737.46039.43
442148-4214836.84938.71
544088-4408838.54540.61
642692-4269237.32439.24
点击查看处理图标(自动生成)
　
原始图谱下载图谱(姜进硙 于 2024-10-08 18:36:56 完成)
生成报告数据部分(等待生成报告)
Current page cost:83 ms