左氨氯地平叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105 对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数5000
标示量(mg)2.5供试品稀释倍数2系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.38 7039670200703787077670358704220.31
216.697335273135732440.21
单位质量响应值RSD%判断
4299.274388.501.46数据可信
供试品溶液-24091402批-左氨氯地平-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min138156-3815688.74490.744.5288.7490.744.52
236950-3695085.94085.94
341182-4118295.78295.78
437367-3736786.90986.91
539861-3986192.71092.71
640566-4056694.35094.35
10min138023-3802388.43593.315.7189.4294.325.68
238382-3838289.27090.22
339273-3927391.34292.41
439005-3900590.71991.68
542897-4289799.771100.80
643135-43135100.325101.37
15min138114-3811488.64793.314.9790.6295.364.96
238777-3877790.18992.14
340102-4010293.27195.35
438717-3871790.04992.02
541913-4191397.48399.62
643089-43089100.218102.38
20min137924-3792488.20593.864.4191.1696.944.39
240067-4006793.18996.14
339557-3955792.00395.12
440186-4018693.46696.44
541122-4112295.64398.86
643275-43275100.650103.93
30min138272-3827289.01492.772.6292.9596.892.67
239760-3976092.47596.46
339844-3984492.67096.81
439812-3981292.59696.61
540077-4007793.21297.50
641550-4155096.638101.03
45min138550-3855089.66191.182.9794.5896.342.99
239037-3903790.79495.81
339011-3901190.73395.90
438295-3829589.06894.11
538820-3882090.28995.61
641508-4150896.541102.01
60min136690-3669085.33590.403.4891.2596.573.45
237871-3787188.08294.10
338929-3892990.54296.72
439641-3964192.19898.23
539902-3990292.80599.13
640169-4016993.42699.97
90min136914-3691485.85689.383.8592.7296.553.78
238317-3831789.11996.12
336833-3683385.66792.85
438320-3832089.12696.18
539620-3962092.14999.50
640576-4057694.373101.95
极限135606-3560682.81488.284.4790.6396.444.32
236071-3607183.89591.88
338279-3827989.03197.16
439123-3912390.99499.04
539466-3946691.791100.17
639184-3918491.13599.76
左氨氯地平叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217 对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数20000
标示量(mg)0.8供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.219682296653966149642096501966020.16
216.259573195862957960.10
单位质量响应值RSD%判断
5959.415895.140.77数据可信
供试品溶液-24091402批-叶酸-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min113488-1348823.34822.523.7123.3522.523.70
212975-1297522.46022.46
313341-1334123.09423.09
412591-1259121.79521.80
513360-1336023.12723.13
612288-1228821.27121.27
10min124220-2422041.92640.592.7642.1940.842.77
223702-2370241.02941.28
323806-2380641.20941.47
423298-2329840.33040.57
523335-2333540.39440.65
622323-2232338.64238.88
15min130126-3012652.14950.773.3452.8751.473.34
229781-2978151.55252.26
330172-3017252.22952.94
428997-2899750.19550.89
529336-2933650.78251.49
627561-2756147.70948.37
20min133693-3369358.32456.273.6659.6357.543.64
233054-3305457.21858.50
333666-3366658.27759.57
431165-3116553.94855.20
532442-3244256.15857.43
631018-3101853.69354.89
30min137582-3758265.05663.623.4667.0165.513.44
236614-3661463.38065.29
338875-3887567.29469.24
435742-3574261.87163.72
536140-3614062.56064.45
635555-3555561.54763.34
45min141698-4169872.18170.924.0574.8673.523.98
239942-3994269.14171.76
343949-4394976.07778.77
440587-4058770.25772.79
539313-3931368.05270.64
640347-4034769.84272.32
60min143354-4335475.04774.294.6978.5277.684.57
240605-4060570.28973.68
346152-4615279.89183.43
443849-4384975.90479.22
541157-4115771.24474.59
642383-4238373.36676.62
90min146045-4604579.70577.884.0184.0282.093.93
243185-4318574.75578.92
347642-4764282.47086.89
445683-4568379.07983.24
543002-4300274.43878.57
644381-4438176.82580.89
极限148413-4841383.80482.982.8289.0088.062.79
246282-4628280.11685.11
349991-4999186.53691.88
447255-4725581.80086.84
546989-4698981.33986.30
648704-4870484.30889.23
点击查看处理图标(人工保存)
　
原始图谱下载图谱(姜进硙 于 2024-10-09 13:45:25 完成)
生成报告数据部分(等待生成报告)
Current page cost:48 ms