叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.111253221125419212540001254164125335712537870.04
210.141249442124958912495160.01
单位质量响应值RSD%判断
124014.54123226.430.46数据可信
供试品溶液-24092401批-5mg规格-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1107278-10727814.24614.471.6114.2514.471.60
2108802-10880214.44814.45
3110776-11077614.71014.71
10min1133804-13380417.76817.662.5717.9317.822.53
2135944-13594418.05318.21
3129262-12926217.16517.33
15min1173434-17343423.03124.357.8223.3924.717.70
2199806-19980626.53326.89
3176912-17691223.49323.85
20min1205962-20596227.35128.313.1227.9628.933.13
2219072-21907229.09229.75
3214446-21444628.47729.09
30min1229160-22916030.43130.025.5931.3530.975.49
2236916-23691631.46132.44
3212211-21221128.18129.11
45min1254659-25465933.81734.036.4635.0735.316.35
2273597-27359736.33237.66
3240638-24063831.95533.20
60min1237583-23758331.55032.956.0033.1834.605.90
2265135-26513535.20936.94
3241685-24168532.09533.69
90min1301518-30151840.04039.435.5142.0241.455.42
2310516-31051641.23543.36
3278822-27882237.02638.98
极限1279725-27972537.14638.877.6339.5741.337.43
2318470-31847042.29144.87
3279914-27991437.17139.54
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.111250604125025712504451250965125019112504920.03
210.141245602124634612459740.05
单位质量响应值RSD%判断
123688.63122877.120.47数据可信
供试品溶液-24092402批-5mg规格-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1111504-11150414.84814.901.1114.8514.901.12
2113309-11330915.08815.09
3110927-11092714.77114.77
10min176473-7647310.18310.685.5410.3510.845.47
285100-8510011.33211.50
378983-7898310.51710.68
15min1178485-17848523.76723.572.6124.0423.852.61
2180709-18070924.06324.36
3171853-17185322.88423.16
20min1128573-12857317.12118.075.4717.6618.625.36
2143388-14338819.09319.65
3135241-13524118.00918.54
30min1216374-21637428.81229.133.5729.5429.873.55
2227470-22747030.29031.06
3212449-21244928.28929.02
45min1162745-16274521.67123.025.5722.7224.095.44
2181876-18187624.21825.33
3174048-17404823.17624.23
60min1247528-24752832.96033.233.8434.2534.553.81
2259928-25992834.61235.99
3241102-24110232.10533.41
90min1188804-18880425.14126.705.2626.8028.405.11
2209241-20924127.86229.63
3203477-20347727.09528.76
极限1287139-28713938.23539.074.3740.1741.074.32
2308162-30816241.03443.11
3285006-28500637.95139.92
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