替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.202694927165270342686427074270170.43
214.102632326292263080.09
单位质量响应值RSD%判断
1902.611865.821.39数据可信
供试品溶液-817010批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min111361-1136142.30445.4417.2342.3045.4417.24
29778-977836.40936.41
313002-1300248.41448.41
414510-1451054.02954.03
514466-1446653.86553.87
610099-1009937.60437.60
10min117388-1738864.74666.3113.3365.1766.7613.36
214529-1452954.10054.46
318672-1867269.52770.01
419762-1976273.58574.13
520726-2072677.17577.71
615767-1576758.71059.09
15min119721-1972173.43374.8213.4274.5075.9413.44
216744-1674462.34863.25
321327-2132779.41380.59
422135-2213582.42183.70
523413-2341387.18088.49
617223-1722364.13165.09
20min121786-2178681.12280.4912.1082.9382.3612.14
217849-1784966.46267.99
323046-2304685.81387.79
423200-2320086.38788.49
524666-2466691.84694.03
619151-1915171.31072.91
30min123698-2369888.24186.7110.5590.8689.3810.63
220349-2034975.77177.96
324382-2438290.78893.62
424828-2482892.44995.41
526215-2621597.614100.71
620255-2025575.42177.74
极限124626-2462691.69790.407.1495.2093.947.34
221866-2186681.42084.37
324522-2452291.30995.05
425371-2537194.47198.36
526584-2658498.988103.06
622702-2270284.53387.60
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.202689626832268452703326803268820.34
214.102663526672266540.10
单位质量响应值RSD%判断
1893.101890.350.11数据可信
供试品溶液-817010批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min121966-2196681.45977.415.8281.4677.415.81
218589-1858968.93668.94
320783-2078377.07277.07
421355-2135579.19479.19
521714-2171480.52580.52
620837-2083777.27377.27
10min126241-2624197.31393.783.2998.1394.553.27
224987-2498792.66393.35
324826-2482692.06592.84
426115-2611596.84697.64
524060-2406089.22590.03
625493-2549394.53995.31
15min126116-2611696.84993.473.5198.6495.183.48
225361-2536194.04995.67
324050-2405089.18890.88
426288-2628897.48799.25
524575-2457591.13592.83
624837-2483792.10693.82
20min125970-2597096.30892.642.6599.0695.282.64
224867-2486792.21894.77
324843-2484392.12994.71
425541-2554194.71797.45
524429-2442990.59393.20
624238-2423889.88592.52
30min125887-2588796.00091.474.0599.7295.053.99
224168-2416889.62593.10
324125-2412589.46692.97
425638-2563895.07798.76
523276-2327686.31789.83
624905-2490592.35895.90
极限124519-2451990.92790.362.9395.6194.852.90
223945-2394588.79893.17
324345-2434590.28294.68
425387-2538794.14698.78
523283-2328386.34390.72
624723-2472391.68396.15
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