叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.051218083121933712209021218241121802212189170.11
29.991227805122772412277640.01
单位质量响应值RSD%判断
121285.27122899.300.94数据可信
供试品溶液-24101701批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min197235-9723513.07412.951.9113.0712.941.88
298649-9864913.26413.26
394196-9419612.66612.67
494429-9442912.69712.70
595504-9550412.84212.84
697652-9765213.13013.13
10min1161667-16166721.73821.511.3521.8821.661.34
2160504-16050421.58221.73
3157586-15758621.18921.33
4162321-16232121.82621.97
5157099-15709921.12421.27
6160669-16066921.60421.75
15min1199923-19992326.88226.342.9027.2726.732.86
2200084-20008426.90427.29
3196217-19621726.38426.76
4198063-19806326.63227.02
5196394-19639426.40726.78
6184861-18486124.85725.24
20min1229108-22910830.80630.310.9831.4930.990.97
2223162-22316230.00730.69
3225187-22518730.27930.95
4226848-22684830.50231.18
5223717-22371730.08130.75
6224673-22467330.21030.87
30min1265152-26515235.65335.301.0736.6836.321.03
2258102-25810234.70535.72
3261712-26171235.19036.20
4262757-26275735.33136.35
5261719-26171935.19136.20
6265853-26585335.74736.74
45min1303365-30336540.79140.301.4242.2141.711.38
2291960-29196039.25740.66
3301618-30161840.55641.95
4302660-30266040.69642.11
5298018-29801840.07241.47
6300880-30088040.45741.85
60min1326554-32655443.90943.341.2945.7945.201.26
2315688-31568842.44844.29
3325771-32577143.80445.65
4323677-32367743.52245.39
5319189-31918942.91944.76
6323246-32324643.46445.31
90min1363317-36331748.85247.941.8351.2250.271.77
2345043-34504346.39548.71
3358344-35834448.18350.52
4357890-35789048.12250.47
5353567-35356747.54149.86
6360922-36092248.53050.86
极限1434043-43404358.36257.970.9461.2760.840.93
2424175-42417557.03559.86
3428672-42867257.64060.51
4433755-43375558.32361.20
5434595-43459558.43661.28
6431518-43151858.02360.89
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.051218029121896712152471215137121401112162780.18
29.991215846121658812162170.05
单位质量响应值RSD%判断
121022.69121743.440.42数据可信
供试品溶液-24101701批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1110691-11069114.97014.815.8714.9714.815.86
2117363-11736315.87215.87
3115828-11582815.66515.66
4108681-10868114.69814.70
5102351-10235113.84213.84
6102340-10234013.84113.84
10min1196176-19617626.53125.415.2526.7025.585.26
2196789-19678926.61426.79
3193342-19334226.14826.32
4189341-18934125.60725.77
5178938-17893824.20024.35
6172873-17287323.38023.53
15min1254224-25422434.38233.135.8434.8433.585.84
2259431-25943135.08635.56
3257843-25784334.87135.34
4240324-24032432.50232.95
5232625-23262531.46131.88
6225263-22526330.46530.88
20min1291825-29182539.46738.594.7640.3139.414.76
2291237-29123739.38840.25
3303275-30327541.01641.87
4282321-28232138.18238.99
5280294-28029437.90838.68
6263258-26325835.60436.36
30min1359949-35994948.68047.955.3149.9649.205.29
2361618-36161848.90650.21
3373387-37338750.49851.81
4352293-35229347.64548.88
5361459-36145948.88550.08
6318722-31872243.10544.25
45min1445136-44513660.20156.747.9262.0258.517.83
2442875-44287559.89661.74
3448745-44874560.68962.56
4423144-42314457.22758.99
5385725-38572552.16653.90
6371479-37147950.24051.87
60min1498212-49821267.37963.058.1269.8765.468.01
2494032-49403266.81469.32
3493250-49325066.70869.25
4474384-47438464.15766.56
5423678-42367857.29959.62
6413797-41379755.96358.15
90min1553715-55371574.88671.756.8378.1374.866.79
2552227-55222774.68577.94
3560489-56048975.80279.09
4548384-54838474.16577.28
5481212-48121265.08068.03
6486943-48694365.85568.66
极限1581311-58131178.61876.623.6182.6980.523.73
2582237-58223778.74382.82
3582203-58220378.73982.87
4572093-57209377.37181.31
5539778-53977873.00176.68
6541408-54140873.22176.76
点击查看处理图标(人工保存)
　
原始图谱下载图谱(谢超君 于 2024-10-19 14:13:33 完成)
生成报告数据部分下载报告(谢超君 于 2024-10-19 14:13:52 完成)
Current page cost:98 ms