二甲双胍恩格列净片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号DC033-12306002对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.99对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.899169591881922429194592288920100.28
29.929207492678923760.47
单位质量响应值RSD%判断
9303.349312.100.07数据可信
供试品溶液-206397批-二甲双胍-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min135536-3553634.01435.3613.8834.0135.3613.88
245207-4520743.27143.27
334824-3482433.33333.33
431521-3152130.17130.17
540954-4095439.20039.20
633618-3361832.17832.18
10min178333-7833374.97873.919.8475.0373.979.84
285674-8567482.00582.08
372511-7251169.40669.46
468955-6895566.00266.05
586644-8664482.93383.00
671196-7119668.14768.20
15min198752-9875294.52391.285.3894.7091.465.39
2100388-10038896.08996.30
390859-9085986.96887.14
491349-9134987.43787.60
5100829-10082996.51196.71
690019-9001986.16486.33
20min1102219-10221997.84196.062.1598.1896.402.17
2102428-10242898.04198.41
398157-9815793.95394.27
497817-9781793.62893.93
5102134-10213497.76098.12
699408-9940895.15195.46
30min1102604-10260498.21097.331.0298.7197.821.04
2102722-10272298.32398.86
3100654-10065496.34396.82
4100210-10021095.91896.38
5101906-10190697.54298.07
6102000-10200097.63298.10
45min1102776-10277698.37497.311.0199.0497.971.03
2102129-10212997.75598.45
3101054-10105496.72697.36
499915-9991595.63696.26
5101883-10188397.52098.21
6102235-10223597.85798.49
60min1102492-10249298.10397.050.9498.9397.870.94
2101636-10163697.28398.14
3100866-10086696.54697.34
499924-9992495.64596.43
5101170-10117096.83797.69
6102250-10225097.87198.67
极限1102358-10235897.97497.140.8498.9798.120.85
2101753-10175397.39598.42
3100665-10066596.35497.31
4100384-10038496.08597.03
5101316-10131696.97797.99
6102424-10242498.03899.00
二甲双胍恩格列净片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100664-202106对照品来源中检所对照品对照品使用方法105℃烘干2小时
对照品含量(%)100对照品水分(%)0对照品稀释倍数20
标示量(mg)500供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.158668368649238665788660418672208663200.11
210.108702238693318697770.08
单位质量响应值RSD%判断
85351.7286116.530.64数据可信
供试品溶液-206397批-恩格列净-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1414253-41425343.48745.0310.9043.4945.0310.90
2503090-50309052.81352.81
3410136-41013643.05543.06
4380172-38017239.91039.91
5468093-46809349.13949.14
6398068-39806841.78841.79
10min1780577-78057781.94380.708.3282.0280.788.32
2834209-83420987.57387.66
3726971-72697176.31676.39
4699726-69972673.45673.52
5852269-85226989.46989.55
6718620-71862075.43975.51
15min1929870-92987097.61694.634.1997.8294.844.20
2936184-93618498.27998.51
3869561-86956191.28591.48
4869872-86987291.31791.51
5940984-94098498.78299.01
6862311-86231190.52390.72
20min1949418-94941899.66898.161.55100.0498.531.57
2948180-94818099.53899.94
3921791-92179196.76897.12
4914727-91472796.02696.37
5943580-94358099.05599.45
6932899-93289997.93498.28
30min1948981-94898199.62298.990.96100.1699.520.97
2949790-94979099.707100.27
3935964-93596498.25598.77
4928951-92895197.51998.02
5942358-94235898.92799.49
6951900-95190099.928100.44
45min1951352-95135299.87198.950.92100.5799.640.92
2944195-94419599.12099.85
3936152-93615298.27598.95
4930553-93055397.68798.35
5940604-94060498.74399.47
6952499-95249999.991100.67
60min1952827-952827100.02698.891.00100.9099.751.01
2942859-94285998.97999.87
3935410-93541098.19799.04
4929010-92901097.52598.35
5939557-93955798.63399.52
6952316-95231699.972100.81
极限1947588-94758899.47698.560.99100.5199.580.99
2941804-94180498.86899.93
3932532-93253297.89598.90
4925412-92541297.14898.14
5936338-93633898.29599.35
6949464-94946499.673100.68
二甲双胍恩格列净片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号DC033-12306002对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.99对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.899256792634925129237692710925600.14
29.929249192995927430.39
单位质量响应值RSD%判断
9358.959349.090.08数据可信
供试品溶液-206397批-二甲双胍-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min136448-3644834.71438.5712.6034.7138.5712.61
242677-4267740.64740.65
347744-4774445.47345.47
444103-4410342.00542.01
537278-3727835.50535.50
634747-3474733.09433.09
10min176495-7649572.85777.217.0472.9177.277.05
282779-8277978.84278.91
389878-8987885.60385.68
483833-8383379.84679.92
579491-7949175.71075.77
673910-7391070.39570.45
15min197892-9789293.23693.152.8993.4293.342.90
299110-9911094.39694.60
399680-9968094.93995.16
499400-9940094.67294.88
598510-9851093.82494.01
692194-9219487.80987.98
20min1103677-10367798.74696.221.5799.0896.561.56
2101035-10103596.22996.59
3100496-10049695.71696.09
4101729-10172996.89097.25
5100110-10011095.34895.69
699079-9907994.36694.69
30min1102987-10298798.08896.351.0498.5996.851.04
2100792-10079295.99896.51
3101122-10112296.31296.85
4101626-10162696.79297.31
5100116-10011695.35495.85
6100302-10030295.53196.01
45min1103629-10362998.70096.291.4299.3696.961.41
2101341-10134196.52197.20
3100310-10031095.53996.24
4101337-10133796.51797.20
599423-9942394.69495.35
6100549-10054995.76696.40
60min1102944-10294498.04896.041.1398.8796.871.12
2100718-10071895.92796.77
3100137-10013795.37496.23
4101157-10115796.34697.19
599810-9981095.06395.88
6100250-10025095.48296.28
极限1102602-10260297.72296.120.9498.7197.110.93
2101009-10100996.20597.20
3100141-10014195.37896.39
4101135-10113596.32597.33
599988-9998895.23296.21
6100660-10066095.87296.83
二甲双胍恩格列净片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100664-202106对照品来源中检所对照品对照品使用方法105℃烘干2小时
对照品含量(%)100对照品水分(%)0对照品稀释倍数20
标示量(mg)500供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.158671648713968705988698088709098699750.20
210.108706158708878707510.03
单位质量响应值RSD%判断
85711.8286212.970.42数据可信
供试品溶液-206397批-恩格列净-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1419577-41957743.92948.5710.6343.9348.5810.63
2484874-48487450.76550.77
3533352-53335255.84155.84
4500137-50013752.36352.36
5433974-43397445.43645.44
6411774-41177443.11243.11
10min1761142-76114279.69083.855.8379.7683.935.83
2814152-81415285.24085.32
3871141-87114191.20791.30
4825397-82539786.41786.50
5791699-79169982.88982.96
6741797-74179777.66577.74
15min1922508-92250896.58596.392.3696.7996.612.37
2928511-92851197.21397.44
3935348-93534897.92998.17
4933728-93372897.75997.99
5926121-92612196.96397.18
6877493-87749391.87292.07
20min1956411-956411100.13498.391.18100.5098.781.18
2940490-94049098.46798.86
3933610-93361097.74798.16
4948911-94891199.34999.74
5931114-93111497.48697.86
6928150-92815097.17597.53
30min1957046-957046100.20198.591.06100.7399.141.06
2939717-93971798.38698.94
3941939-94193998.61999.19
4948518-94851899.30899.87
5930908-93090897.46498.00
6931985-93198597.57798.09
45min1960864-960864100.60098.471.27101.3099.181.26
2942204-94220498.64799.36
3932983-93298397.68198.42
4945744-94574499.01799.74
5928354-92835497.19797.90
6933020-93302097.68598.36
60min1953851-95385199.86698.121.17100.7398.991.16
2936754-93675498.07698.96
3930407-93040797.41298.31
4945277-94527798.96899.86
5923487-92348796.68797.55
6933020-93302097.68598.53
极限1950791-95079199.54698.030.95100.5899.070.94
2935224-93522497.91698.96
3929073-92907397.27298.33
4942651-94265198.69499.75
5927707-92770797.12998.15
6932640-93264097.64598.65
点击查看处理图标(人工保存)
　
原始图谱下载图谱(姜进硙 于 2024-10-22 19:20:40 完成)
生成报告数据部分(等待生成报告)
Current page cost:58 ms