贝派度酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.21 3054293059343062233059343059733058990.10
210.163055773058513057140.07
单位质量响应值RSD%判断
29960.7230089.960.31数据可信
影响因素30天-供试品溶液-2024090421批-pH6.6
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1112450-11245037.34734.5627.2337.3534.5627.24
2119234-11923439.60039.60
3137204-13720445.56845.57
4102139-10213933.92333.92
5100324-10032433.32033.32
653084-5308417.63017.63
10min1231550-23155076.90374.995.6376.9675.055.64
2229854-22985476.33976.41
3240659-24065979.92880.00
4224284-22428474.48974.55
5225674-22567474.95175.01
6202702-20270267.32267.35
15min1263997-26399787.67985.454.1087.8785.644.12
2256423-25642385.16385.36
3268745-26874589.25689.47
4259401-25940186.15386.33
5257286-25728685.45085.63
6237932-23793279.02279.16
20min1280329-28032993.10390.173.6093.4490.493.61
2268226-26822689.08389.42
3279906-27990692.96393.32
4274969-27496991.32391.65
5271408-27140890.14090.46
6254070-25407084.38284.66
30min1288247-28824795.73394.382.0396.2294.862.05
2280414-28041493.13193.62
3288725-28872595.89296.40
4288338-28833895.76396.24
5285037-28503794.66795.14
6274340-27434091.11491.53
45min1296048-29604898.32497.520.9398.9898.150.94
2289300-28930096.08396.72
3293794-29379497.57598.25
4296091-29609198.33898.97
5294958-29495897.96298.59
6291499-29149996.81397.38
60min1300177-30017799.69598.820.92100.5199.610.93
2295594-29559498.17398.97
3296020-29602098.31499.15
4299397-29939799.436100.24
5300164-30016499.691100.48
6293868-29386897.60098.33
极限1306957-306957101.947100.561.12102.93101.521.13
2300969-30096999.958100.92
3301818-301818100.240101.24
4301840-301840100.247101.21
5306743-306743101.876102.84
6298419-29841999.111100.00
贝派度酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.21 3057343058083053903058133058253057140.07
210.163052553055933054240.08
单位质量响应值RSD%判断
29942.6130061.420.29数据可信
影响因素30天-供试品溶液-2024090421批-pH6.6
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1121885-12188540.51234.0625.2340.5134.0625.23
2121327-12132740.32740.33
3105506-10550635.06835.07
4111491-11149137.05737.06
552277-5227717.37617.38
6102380-10238034.02934.03
10min1237597-23759778.97276.484.7579.0476.544.77
2238301-23830179.20679.27
3233668-23366877.66677.72
4230353-23035376.56576.63
5208723-20872369.37569.40
6232027-23202777.12177.18
15min1269806-26980689.67888.053.2089.8888.233.21
2270197-27019789.80890.01
3268683-26868389.30589.49
4261444-26144486.89987.09
5249028-24902882.77282.92
6270221-27022189.81690.00
20min1287912-28791295.69693.122.8796.0493.452.88
2283699-28369994.29694.64
3283410-28341094.20094.54
4275615-27561591.60991.94
5266004-26600488.41488.70
6284278-28427894.48894.82
30min1293042-29304297.40197.041.9397.9197.521.94
2295968-29596898.37498.88
3294907-29490798.02198.51
4288909-28890996.02796.51
5282061-28206193.75194.18
6296854-29685498.66899.16
45min1299056-29905699.40099.561.34100.07100.211.35
2302729-302729100.621101.29
3301682-301682100.273100.93
4297654-29765498.93499.58
5292739-29273997.30097.89
6303355-303355100.829101.49
60min1302408-302408100.514100.781.04101.35101.591.06
2305361-305361101.496102.33
3305351-305351101.492102.32
4302337-302337100.490101.30
5297672-29767298.94099.69
6306071-306071101.732102.56
极限1307555-307555102.225102.070.61103.23103.050.64
2308358-308358102.492103.50
3308279-308279102.465103.46
4306509-306509101.877102.86
5303568-303568100.900101.81
6308251-308251102.456103.45
点击查看处理图标(人工保存)
　
原始图谱下载图谱(姜进硙 于 2024-10-23 17:00:41 完成)
生成报告数据部分(等待生成报告)
Current page cost:77 ms