磷酸奥司他韦干糖浆项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号101096-202103对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.7对照品水分(%)0对照品稀释倍数100
标示量(mg)75供试品稀释倍数1系数0.7612
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.051543440154411115499571547067154773015464610.18
210.001538095154375915409270.26
单位质量响应值RSD%判断
153876.72154092.700.10数据可信
供试品溶液-24101501批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11523595-152359590.10994.013.7890.1194.013.77
21508676-150867689.22689.23
31661835-166183598.28598.28
41615743-161574395.55995.56
51614456-161445695.48395.48
61613054-161305495.40095.40
10min11660952-166095298.23299.241.0799.23100.281.09
21674445-167444599.030100.02
31705112-1705112100.844101.94
41668754-166875498.69499.76
51663766-166376698.39999.46
61694521-1694521100.218101.28
15min11637453-163745396.84398.181.2098.94100.321.21
21648742-164874297.51099.60
31692517-1692517100.099102.31
41653651-165365197.80199.96
51654021-165402197.82399.98
61673608-167360898.981101.15
20min11624859-162485996.09896.881.1699.27100.121.18
21626444-162644496.19299.37
31669588-166958898.743102.07
41627107-162710796.23199.48
51626902-162690296.21999.46
61653934-165393497.817101.09
30min11606851-160685195.03395.931.0199.27100.241.03
21611884-161188495.33099.57
31648577-164857797.501101.92
41615442-161544295.54199.86
51613651-161365195.43599.75
61635287-163528796.715101.07
极限11513936-151393689.53892.322.6694.8397.702.56
21546517-154651791.46496.77
31616851-161685195.624101.13
41585959-158595993.79799.17
51585006-158500693.74199.11
61518081-151808189.78395.22
磷酸奥司他韦干糖浆项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号101096-202103对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.7对照品水分(%)0对照品稀释倍数100
标示量(mg)75供试品稀释倍数1系数0.7612
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.051559149155867615538801555199155666615567140.15
210.001546455154743615469460.05
单位质量响应值RSD%判断
154896.92154694.600.10数据可信
供试品溶液-24101502批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11522490-152249089.57285.434.1089.5785.434.10
21492935-149293587.83387.83
31422532-142253283.69183.69
41368270-136827080.49980.50
51492815-149281587.82687.83
61413362-141336283.15183.15
10min11545891-154589190.94890.491.1291.9491.441.12
21528057-152805789.89990.88
31534555-153455590.28291.21
41513680-151368089.05389.95
51542093-154209390.72591.70
61564370-156437092.03692.96
15min11521687-152168789.52489.190.6691.5391.140.67
21507405-150740588.68490.66
31525540-152554089.75191.68
41502172-150217288.37690.26
51512754-151275488.99990.98
61526064-152606489.78291.73
20min11511998-151199888.95488.480.6091.9591.420.60
21497042-149704288.07591.03
31510210-151021088.84991.78
41492033-149203387.78090.65
51498995-149899588.18991.16
61512876-151287689.00691.95
30min11493213-149321387.84987.360.8891.8491.280.86
21470581-147058186.51890.46
31480892-148089287.12491.04
41475357-147535786.79990.64
51482720-148272087.23291.18
61506279-150627988.61892.55
极限11479341-147934187.03385.422.7092.0090.322.56
21374070-137407080.84085.74
31471236-147123686.55691.44
41453788-145378885.53090.34
51463147-146314786.08091.00
61470383-147038386.50691.42
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