非奈利酮片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号FN-706-231101对照品来源自制对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 11.163783533781053780163780993780343781210.04
2 11.193772903769393771140.07
单位质量响应值RSD%判断
33881.8133700.980.38数据可信
供试品溶液-24101601批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1141586-14158637.71037.6029.2137.7137.6029.21
267649-6764918.01818.02
3195584-19558452.09252.09
4150291-15029140.02940.03
5147416-14741639.26339.26
6144437-14443738.47038.47
10min1225000-22500059.92760.0716.8659.9960.1316.88
2157473-15747341.94241.97
3267977-26797771.37471.46
4229218-22921861.05061.12
5220493-22049358.72758.79
6253039-25303967.39567.46
15min1264879-26487970.54870.2111.3670.7170.3811.38
2211153-21115356.23956.34
3294625-29462578.47178.68
4265408-26540870.68970.86
5255619-25561968.08268.25
6290070-29007077.25877.43
20min1289348-28934877.06576.607.7977.3576.887.82
2248770-24877066.25866.45
3309383-30938382.40282.74
4290231-29023177.30177.59
5279180-27918074.35774.63
6308603-30860382.19482.50
30min1317288-31728884.50783.704.1884.9284.104.22
2293687-29368778.22178.53
3326224-32622486.88787.36
4315795-31579584.10984.52
5304539-30453981.11181.51
6327912-32791287.33787.78
45min1333655-33365588.86688.502.7489.4289.052.77
2322156-32215685.80486.24
3339104-33910490.31890.94
4335792-33579289.43589.99
5320351-32035185.32385.86
6342579-34257991.24391.83
60min1342501-34250191.22291.022.3991.9291.722.42
2336223-33622389.55090.13
3346809-34680992.37093.14
4346314-34631492.23892.94
5328279-32827987.43488.11
6350380-35038093.32194.06
极限1350801-35080193.43392.951.9694.2893.801.98
2344790-34479091.83292.56
3350912-35091293.46394.39
4352386-35238693.85594.71
5337724-33772489.95090.77
6357312-35731295.16796.06
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