叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.091194416119457011942751195048119338111943380.06
210.041190202119083011905160.04
单位质量响应值RSD%判断
118368.48118577.290.13数据可信
供试品溶液-24102102批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min167990-679909.42110.517.869.4210.517.86
277960-7796010.80210.80
381281-8128111.26311.26
472647-7264710.06610.07
583262-8326211.53711.54
671777-717779.9469.95
10min1139282-13928219.29919.094.7919.4019.204.79
2135647-13564718.79618.92
3142063-14206319.68519.81
4132037-13203718.29618.41
5147571-14757120.44820.58
6129830-12983017.99018.10
15min11-10.00020.3449.290.3220.6748.54
2177066-17706624.53524.86
3182088-18208825.23125.57
4169407-16940723.47423.79
5186845-18684525.89026.25
6165231-16523122.89523.21
20min1196291-19629127.19927.693.5927.5228.243.74
2198462-19846227.50028.10
3208336-20833628.86829.49
4194402-19440226.93727.51
5209064-20906428.96929.61
6192364-19236426.65527.22
30min1240039-24003933.26132.602.4633.8833.462.37
2234097-23409732.43733.34
3234670-23467032.51733.46
4236362-23636232.75133.63
5241329-24132933.43934.40
6225036-22503631.18232.04
45min1290579-29057940.26437.913.6341.2539.143.32
2261189-26118936.19137.46
3274793-27479338.07639.38
4269182-26918237.29938.54
5276704-27670438.34139.68
6269124-26912437.29138.50
60min1315852-31585243.76641.214.5545.2042.854.26
2279616-27961638.74540.41
3293757-29375740.70442.43
4307847-30784742.65644.31
5301040-30104041.71343.48
6286305-28630539.67141.29
90min1370022-37002251.27246.136.7553.2048.246.33
2303224-30322442.01644.12
3329372-32937245.63947.82
4343647-34364747.61749.74
5329405-32940545.64347.87
6321958-32195844.61246.67
极限1406698-40669856.35353.343.4758.8555.963.28
2371005-37100551.40853.97
3381617-38161752.87855.57
4391928-39192854.30756.96
5386142-38614253.50556.24
6372313-37231351.58954.15
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.091180503118193511832141184299118389311827690.14
210.041186870118653011867000.03
单位质量响应值RSD%判断
117221.90118197.210.59数据可信
供试品溶液-24102401批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min188974-8897412.40912.601.7412.4112.601.74
290992-9099212.69012.69
388593-8859312.35612.36
490219-9021912.58212.58
592981-9298112.96812.97
690359-9035912.60212.60
10min1156346-15634621.80522.381.4621.9422.521.46
2159488-15948822.24322.38
3161190-16119022.48022.62
4162539-16253922.66822.81
5162552-16255222.67022.81
6160512-16051222.38622.53
15min1201393-20139328.08729.102.1528.4729.492.13
2207592-20759228.95229.34
3210754-21075429.39329.78
4214443-21444329.90730.30
5210929-21092929.41729.81
6206974-20697428.86529.25
20min1222331-22233131.00733.634.0631.7034.354.00
2243258-24325833.92634.64
3248339-24833934.63435.35
4248960-24896034.72135.45
5243461-24346133.95434.68
6240572-24057233.55134.26
30min1273013-27301338.07640.072.9539.1141.152.93
2288930-28893040.29541.38
3295455-29545541.20542.30
4287709-28770940.12541.23
5295535-29553541.21742.32
6283135-28313539.48740.57
45min1316004-31600444.07147.153.4845.5348.683.45
2340832-34083247.53449.07
3348042-34804248.53950.10
4341862-34186247.67849.23
5346631-34663148.34349.90
6335042-33504246.72648.25
60min1349015-34901548.67552.404.1750.6254.454.12
2378059-37805952.72654.79
3391946-39194654.66256.76
4386481-38648153.90055.99
5382191-38219153.30255.40
6366568-36656851.12353.16
90min1389006-38900654.25258.704.2156.7461.344.16
2423983-42398359.13061.78
3436688-43668860.90263.61
4432708-43270860.34763.03
5430123-43012359.98762.67
6412994-41299457.59860.21
极限1462743-46274364.53666.012.1067.6369.302.13
2465810-46581064.96468.27
3488738-48873868.16271.54
4479357-47935766.85370.21
5476294-47629466.42669.78
6466840-46684065.10868.36
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