诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.18 3942634394048039429523941754394234639420330.03
210.13 3942373393981239410920.05
单位质量响应值RSD%判断
387233.10389051.530.34数据可信
供试品溶液-24022901批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13636338-363633883.98088.334.3883.9888.334.38
23765451-376545186.96286.96
34113865-411386595.00995.01
43705730-370573085.58385.58
53870041-387004189.37889.38
63857671-385767189.09289.09
10min14153506-415350695.92498.852.1496.0699.002.14
24319557-431955799.75999.90
34413266-4413266101.923102.08
44221368-422136897.49197.63
54250117-425011798.15598.30
64324531-432453199.874100.02
15min14260644-426064498.39999.651.2998.7099.961.29
24328870-432887099.974100.29
34407930-4407930101.800102.13
44302220-430222099.35999.66
54258835-425883598.35798.67
64330503-4330503100.012100.33
20min14268454-426845498.57999.641.2499.04100.121.24
24333623-4333623100.084100.56
34401650-4401650101.655102.15
44308903-430890399.51399.98
54251002-425100298.17698.65
64322399-432239999.825100.31
30min14261879-426187998.42799.621.2099.06100.271.20
24340969-4340969100.254100.90
34393787-4393787101.473102.14
44307129-430712999.472100.11
54256622-425662298.30698.95
64322095-432209599.818100.47
诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.18 3934922393322939344613933847393104039335000.04
210.13 3922227392657339244000.08
单位质量响应值RSD%判断
386394.89387403.750.19数据可信
供试品溶液-24022901批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13685189-368518985.38280.985.4085.3880.985.40
23729074-372907486.39886.40
33344045-334404577.47877.48
43390612-339061278.55778.56
53270791-327079175.78075.78
63550408-355040882.25982.26
10min14141322-414132295.95092.145.2196.0992.275.21
24129584-412958495.67895.82
33892685-389268590.18990.32
43866333-386633389.57989.71
53653113-365311384.63884.76
64177055-417705596.77896.91
15min14182472-418247296.90396.411.4197.2196.701.41
24215171-421517197.66197.96
34086403-408640394.67794.96
44130899-413089995.70895.99
54118623-411862395.42495.69
64234342-423434298.10598.40
20min14206686-420668697.46497.061.1297.9397.511.13
24225573-422557397.90298.37
34140397-414039795.92896.37
44207783-420778397.49097.93
54120768-412076895.47395.90
64233166-423316698.07898.54
30min14194808-419480897.18997.401.2097.8298.011.21
24255311-425531198.59199.22
34165863-416586396.51897.12
44214252-421425297.63998.24
54132099-413209995.73696.32
64260191-426019198.70499.33
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