诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.183933433393396039319263931892393319039328800.03
210.13 3922011392679739244040.09
单位质量响应值RSD%判断
386333.99387404.150.20数据可信
供试品溶液-24022901批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11105544-110554425.61624.893.8225.6224.893.82
21044396-104439624.19924.20
31027995-102799523.81923.82
41043598-104359824.18124.18
51129783-112978326.17826.18
61093210-109321025.33025.33
10min12271232-227123252.62651.201.8752.6751.241.86
22158249-215824950.00850.05
32223286-222328651.51551.55
42192853-219285350.81050.85
52233536-223353651.75351.80
62178410-217841050.47550.52
15min13092791-309279171.66269.971.8971.7970.101.88
23037823-303782370.38870.51
33063141-306314170.97571.10
42987332-298733269.21869.34
53004465-300446569.61569.75
62934299-293429967.99068.12
20min13616545-361654583.79882.301.6784.0582.551.67
23581756-358175682.99283.23
33591753-359175383.22383.47
43515394-351539481.45481.69
53552411-355241182.31282.56
63454787-345478780.05080.29
30min14066667-406666794.22793.681.0694.6294.061.05
24093748-409374894.85595.23
34064456-406445694.17694.56
44016848-401684893.07393.45
54041194-404119493.63794.02
63974136-397413692.08392.46
45min14183814-418381496.94297.321.0397.4997.851.03
24267918-426791898.89199.43
34234062-423406298.10698.65
44173200-417320096.69697.23
54190361-419036197.09397.63
64150182-415018296.16396.69
60min14188362-418836297.04797.371.2897.7698.071.28
24267100-426710098.87299.57
34255694-425569498.60799.31
44173486-417348696.70297.39
54207328-420732897.48798.19
64122649-412264995.52596.21
极限14138563-413856395.89397.321.3996.7698.181.39
24262859-426285998.77399.64
34272430-427243098.99599.86
44208579-420857997.51698.37
54175987-417598796.76097.62
64141582-414158295.96396.81
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