非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.291946802194191819398431939070193842219412110.18
210.431991056198407719875660.25
单位质量响应值RSD%判断
188650.24190562.420.72数据可信
供试品溶液-2024092212批-pH6.0
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1480398-48039822.80431.3138.9422.8031.3138.94
2950395-95039545.11345.11
3823342-82334239.08239.08
4415174-41517419.70719.71
5895266-89526642.49642.50
6393123-39312318.66118.66
10min11431504-143150467.95172.1314.7668.0072.2014.78
21786881-178688184.82084.92
31759708-175970883.53083.62
41270994-127099460.33260.38
51572084-157208474.62474.72
61296461-129646161.54061.58
15min11900977-190097790.23689.665.1990.4489.895.22
21981757-198175794.07094.36
32005789-200578995.21195.48
41752726-175272683.19883.38
51886538-188653889.55089.81
61805173-180517385.68885.87
20min12036744-203674496.68095.302.8697.0895.732.90
22031200-203120096.41796.91
32083126-208312698.88299.37
41914983-191498390.90091.26
51998484-199848494.86495.32
61981575-198157594.06194.43
30min12114437-2114437100.36898.301.89100.9998.941.91
22059065-205906597.74098.45
32120371-2120371100.650101.35
42019367-201936795.85596.42
52059952-205995297.78298.45
62051742-205174297.39297.97
45min12137314-2137314101.45499.031.82102.2999.891.83
22068321-206832198.17999.11
32129506-2129506101.083102.01
42045275-204527597.08597.86
52074358-207435898.46699.35
62062687-206268797.91298.71
60min12136083-2136083101.39699.021.84102.46100.101.84
22060372-206037297.80298.95
32132464-2132464101.224102.38
42048540-204854097.24098.23
52069581-206958198.23999.35
62068625-206862598.19399.21
极限12138403-2138403101.50698.961.91102.80100.261.92
22062379-206237997.89799.26
32129901-2129901101.102102.48
42039762-203976296.82398.03
52070597-207059798.28799.61
62068181-206818198.17299.40
非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.291952971195184519507081949897194894419508730.09
210.432003347200350720034270.01
单位质量响应值RSD%判断
189589.21192083.130.93数据可信
供试品溶液-2024092212批-pH6.0
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1740425-74042534.92136.6125.2634.9236.6125.25
2737201-73720134.76934.77
3420598-42059819.83719.84
4945660-94566044.60044.60
5906583-90658342.75742.76
6907281-90728142.79042.79
10min11469772-146977269.31974.5913.4569.4074.6713.47
21500171-150017170.75270.83
31246412-124641258.78458.83
41773785-177378583.65783.76
51722854-172285481.25581.35
61776107-177610783.76683.86
15min11829112-182911286.26688.845.5086.5089.095.54
21873650-187365088.36788.60
31709122-170912280.60780.78
41986488-198648893.68993.97
51941267-194126791.55691.83
61962547-196254792.55992.84
20min11984564-198456493.59894.162.2794.0294.612.31
21989432-198943293.82794.26
31921085-192108590.60490.96
42054492-205449296.89697.39
52003134-200313494.47494.95
62026766-202676695.58896.08
30min12035600-203560096.00596.531.0596.6497.191.08
22031537-203153795.81396.45
32033904-203390495.92596.48
42084344-208434498.30499.01
52034855-203485595.97096.66
62060672-206067297.18797.89
45min12043397-204339796.37297.131.0797.2298.001.08
22040069-204006996.21697.07
32065756-206575697.42798.20
42096839-209683998.89399.82
52043363-204336396.37197.27
62067094-206709497.49098.41
60min12042584-204258496.33496.961.0297.3998.051.03
22037858-203785896.11197.18
32063551-206355197.32398.31
42092213-209221398.67599.82
52039034-203903496.16797.28
62060297-206029797.17098.30
极限12039950-203995096.21096.800.9497.4898.100.95
22031869-203186995.82997.11
32063252-206325297.30998.51
42081874-208187498.18799.55
52037124-203712496.07797.41
62060125-206012597.16198.51
非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.291953011195468119530771950435195087119524150.09
210.432008696200837120085340.02
单位质量响应值RSD%判断
189739.07192572.771.05数据可信
供试品溶液-2024092213批-pH6.0
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1797932-79793237.57032.7022.6337.5732.7022.64
2835043-83504339.31839.32
3759745-75974535.77235.77
4511469-51146924.08224.08
5477535-47753522.48522.48
6784935-78493536.95836.96
10min11735792-173579281.72971.6011.9481.8171.6811.95
21559950-155995073.45073.54
31537555-153755572.39572.47
41284441-128444160.47760.53
51329844-132984462.61562.67
61676957-167695778.95979.04
15min12003330-200333094.32688.855.1094.5989.085.13
21912114-191211490.03190.28
31888356-188835688.91289.15
41778150-177815083.72383.91
51770800-177080083.37783.57
61969265-196926592.72292.98
20min12063745-206374597.17195.012.0497.6595.442.07
22041286-204128696.11396.56
31995111-199511193.93994.38
42004111-200411194.36394.74
51953934-195393492.00092.37
62049441-204944196.49796.96
30min12089532-208953298.38597.910.5899.0898.550.60
22095418-209541898.66299.33
32063940-206394097.18097.83
42079725-207972597.92398.51
52068469-206846997.39397.97
62079358-207935897.90698.58
45min12094019-209401998.59698.390.4699.5199.250.48
22105037-210503799.115100.00
32076029-207602997.74998.61
42088281-208828198.32699.13
52086478-208647898.24199.04
62088152-208815298.32099.22
60min12098036-209803698.78598.420.3899.9199.490.40
22099320-209932098.84699.95
32077576-207757697.82298.90
42090211-209021198.41799.44
52087727-208772798.30099.31
62088576-208857698.34099.45
极限12093677-209367798.58098.110.4999.9399.410.51
22096209-209620998.699100.02
32068007-206800797.37198.67
42082814-208281498.06899.31
52081968-208196898.02999.26
62080131-208013197.94299.27
非布司他片项目信息
介质体积(ml)900取样体积(ml)2补液体积(ml)2
对照品批号101278-202104对照品来源中检院对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.291968441196797619679211968015196714019678990.03
210.432019551201917520193630.02
单位质量响应值RSD%判断
191243.83193611.030.87数据可信
供试品溶液-2024092213批-pH6.0
时间
(分钟)
样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)
平均(%)RSD%
5min1756652-75665235.39136.2922.2635.3936.2922.26
2757107-75710735.41235.41
3590881-59088127.63727.64
41033841-103384148.35548.36
5911607-91160742.63842.64
6605256-60525628.30928.31
10min11448509-144850967.75174.3512.0267.8374.4312.03
21721544-172154480.52180.60
31399871-139987165.47665.54
41784037-178403783.44483.55
51780812-178081283.29383.39
61402866-140286665.61665.68
15min11802364-180236484.30189.285.1384.5389.535.15
21991965-199196593.16993.43
31809164-180916484.61984.83
41976134-197613492.42992.72
52019154-201915494.44194.72
61854075-185407586.72086.93
20min11977942-197794292.51494.372.2592.9394.812.28
22058840-205884096.29796.76
31974297-197429792.34392.74
42047672-204767295.77596.27
52069034-206903496.77497.26
61978149-197814992.52392.92
30min12049008-204900895.83896.551.4396.4697.201.46
22097800-209780098.12098.80
32048475-204847595.81396.41
42066569-206656996.65997.37
52098602-209860298.15798.86
62025274-202527494.72795.33
45min12055972-205597296.16396.841.3297.0097.711.35
22101642-210164298.29999.20
32055360-205536096.13596.95
42074506-207450697.03097.96
52101220-210122098.28099.20
62033878-203387895.13095.95
60min12053292-205329296.03896.611.3097.0997.701.33
22097298-209729898.09699.21
32054663-205466396.10297.13
42065516-206551696.61097.75
52095134-209513497.99599.14
62027691-202769194.84095.87
极限12046742-204674295.73296.621.3196.9997.921.34
22099377-209937798.19399.53
32057235-205723596.22297.46
42068659-206865996.75798.11
52093091-209309197.89999.26
62029598-202959894.93096.17
点击查看处理图标(自动生成)
 
原始图谱下载图谱(谢超君 于 2024-10-30 11:42:05 完成)
生成报告数据部分下载报告(谢超君 于 2024-10-30 11:44:19 完成)
Current page cost:81 ms