苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.608691786919870158705587297870410.18
214.678714087214871770.07
单位质量响应值RSD%判断
5961.715942.540.23数据可信
供试品溶液-2024101922批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min162821-6282174.05371.0113.0174.0571.0113.01
250146-5014659.11259.11
359241-5924169.83369.83
452479-5247961.86261.86
569919-6991982.42082.42
666831-6683178.78078.78
10min171922-7192284.78181.706.4386.2683.126.54
263115-6311574.40075.58
368557-6855780.81582.21
465147-6514776.79578.03
573823-7382387.02288.67
673262-7326286.36187.94
15min171273-7127384.01680.915.7487.1983.965.87
262597-6259773.78976.46
368400-6840080.62983.64
465436-6543677.13579.91
572552-7255285.52488.91
671548-7154884.34087.64
20min171505-7150584.29080.584.7089.1585.264.87
264323-6432375.82379.97
368140-6814080.32384.95
464727-6472776.30080.62
571368-7136884.12889.23
670088-7008882.61987.61
30min170288-7028882.85580.594.1589.4086.874.37
264670-6467076.23381.90
367728-6772879.83786.07
465478-6547877.18583.03
571152-7115283.87390.66
670863-7086383.53390.17
45min169181-6918181.55080.333.0389.7588.233.30
265116-6511676.75883.95
367193-6719379.20787.04
467100-6710079.09786.48
569446-6944681.86290.32
670845-7084583.51291.82
60min168567-6856780.82678.953.2690.6688.453.53
264020-6402075.46684.19
366295-6629578.14887.56
465044-6504476.67385.64
568555-6855580.81290.91
669375-6937581.77991.76
极限175281-7528188.74188.201.28100.1999.291.04
275295-7529588.75798.99
374090-7409087.33798.31
475592-7559289.10799.61
573216-7321686.30698.02
675485-7548588.981100.60
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.608755087063872418753187224873220.25
214.678761387361874870.21
单位质量响应值RSD%判断
5980.965963.670.21数据可信
供试品溶液-2024101923批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min168223-6822380.14975.946.4880.1575.946.48
257762-5776267.85967.86
368446-6844680.41180.41
462201-6220173.07473.07
563983-6398375.16875.17
667211-6721178.96078.96
10min172427-7242785.08881.774.1786.6983.294.21
265073-6507376.44877.81
371989-7198984.57386.18
467425-6742579.21180.67
569358-6935881.48282.99
671365-7136583.84085.42
15min172271-7227184.90582.332.8888.2185.492.95
267807-6780779.66082.55
371737-7173784.27787.58
468166-6816680.08283.13
568866-6886680.90484.04
671635-7163584.15787.41
20min170755-7075583.12380.383.5088.1385.183.55
265240-6524076.64481.12
370903-7090383.29788.28
465966-6596677.49782.14
568286-6828680.22384.97
669357-6935781.48186.42
30min169175-6917581.26779.353.2187.9385.763.27
264579-6457975.86881.88
369545-6954581.70288.35
465890-6589077.40883.61
566494-6649478.11884.47
669580-6958081.74388.31
45min168556-6855680.54079.522.8888.8387.512.82
267004-6700478.71786.25
367569-6756979.38187.67
466865-6686578.55386.30
565169-6516976.56184.48
670945-7094583.34791.55
60min166842-6684278.52679.471.1788.4389.051.15
267738-6773879.57988.68
368831-6883180.86390.74
467932-6793279.80789.12
566692-6669278.35087.80
667812-6781279.66689.54
极限171473-7147383.96789.073.0995.44100.252.56
277516-7751691.066101.76
376078-7607889.377100.87
477994-7799491.628102.54
575312-7531288.47799.49
676548-7654889.929101.39
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.608752387561869038741487451873700.31
214.678678086467866240.26
单位质量响应值RSD%判断
5984.255904.840.95数据可信
供试品溶液-2024102021批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min164261-6426175.85075.405.8575.8575.405.85
270997-7099783.80183.80
363643-6364375.12175.12
460525-6052571.44071.44
562051-6205173.24273.24
661811-6181172.95872.96
10min172029-7202985.01981.575.1586.5483.085.15
274289-7428987.68789.36
369470-6947081.99983.50
465060-6506076.79378.22
567741-6774179.95881.42
666053-6605377.96579.42
15min172060-7206085.05681.894.4988.2785.034.52
273644-7364486.92590.36
369561-6956182.10685.25
465013-6501376.73879.70
568302-6830280.62083.68
667701-6770179.91182.93
20min172107-7210785.11181.064.6590.0385.844.66
272800-7280085.92991.10
368287-6828780.60285.39
464766-6476676.44680.95
567818-6781880.04984.73
666250-6625078.19882.81
30min170322-7032283.00480.513.4989.6286.913.58
271885-7188584.84991.74
367240-6724079.36685.76
466060-6606077.97484.00
567653-6765379.85486.13
666109-6610978.03184.21
45min171393-7139384.26880.773.3892.5588.783.46
270942-7094283.73692.32
368155-6815580.44688.43
465582-6558277.40985.00
567771-6777179.99387.87
666732-6673278.76786.51
60min169830-6983082.42480.623.0492.3990.243.06
270128-7012882.77593.03
370103-7010382.74692.34
467681-6768179.88789.02
566990-6699079.07188.55
665075-6507576.81186.13
极限179583-7958393.93590.682.22105.55101.922.15
276344-7634490.112102.03
376478-7647890.270101.52
478003-7800392.071102.80
575729-7572989.386100.44
674832-7483288.32899.18
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