苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.608677186382865918672586723866380.19
214.678655986847867030.24
单位质量响应值RSD%判断
5934.115910.220.29数据可信
供试品溶液-2024101922批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min181246-8124696.25799.462.1396.2699.462.13
283057-8305798.40298.40
383544-8354498.97998.98
484137-8413799.68299.68
586296-86296102.240102.24
685402-85402101.181101.18
10min184050-8405099.579102.801.77100.54103.801.76
287525-87525103.696104.68
386394-86394102.356103.35
488326-88326104.645105.64
587813-87813104.037105.06
686525-86525102.511103.52
15min184021-8402199.545101.971.68101.50103.991.67
287289-87289103.416105.44
386525-86525102.511104.52
487197-87197103.307105.35
586905-86905102.961105.02
684470-84470100.076102.11
20min184047-8404799.575101.061.39102.53104.101.38
287067-87067103.153106.21
384607-84607100.239103.28
486433-86433102.402105.48
585029-85029100.739103.83
684615-84615100.248103.29
30min181190-8119096.19098.551.37100.14102.601.36
284475-84475100.082104.17
383208-8320898.581102.62
482756-8275698.046102.15
583647-8364799.101103.20
683809-8380999.293103.33
45min180847-8084795.78497.662.63100.70102.692.54
285002-85002100.707105.79
380419-8041995.277100.30
484361-8436199.947105.03
583700-8370099.164104.25
680236-8023695.060100.09
60min180511-8051195.38697.301.27101.26103.321.24
282974-8297498.304104.40
382952-8295298.278104.26
481175-8117596.173102.25
582411-8241197.637103.72
682746-8274698.034104.02
极限179742-7974294.47596.132.76101.30103.122.59
283152-8315298.515105.59
383527-8352798.959105.92
477535-7753591.86098.90
581213-8121396.218103.28
681674-8167496.764103.73
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.608642886462865678640586529864780.08
214.678652986677866030.13
单位质量响应值RSD%判断
5923.155903.410.24数据可信
供试品溶液-2024101923批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min183971-8397199.63598.791.9499.6398.791.93
281658-8165896.89096.89
381689-8168996.92796.93
482807-8280798.25498.25
583518-8351899.09799.10
685925-85925101.953101.95
10min185615-85615101.585101.222.06102.58102.202.05
284900-84900100.737101.71
382101-8210197.41698.39
485585-85585101.550102.53
587124-87124103.376104.37
686496-86496102.631103.65
15min185115-85115100.992100.380.94103.00102.380.95
284825-84825100.648102.62
383629-8362999.229101.17
483610-8361099.206101.20
585475-85475101.419103.44
684967-84967100.816102.86
20min183527-8352799.10898.561.80102.13101.561.78
282842-8284298.295101.28
380410-8041095.40998.35
483046-8304698.537101.53
584915-84915100.755103.79
683650-8365099.254102.31
30min181396-8139696.57996.711.83100.59100.701.81
281078-8107896.202100.17
378852-7885293.56197.45
482509-8250997.900101.88
583046-8304698.537102.58
682153-8215397.478101.52
45min182907-8290798.37295.991.84103.35100.951.79
279143-7914393.90698.83
379618-7961894.47099.30
480998-8099896.107101.06
580422-8042295.424100.46
682328-8232897.685102.71
60min180384-8038495.37994.861.71101.34100.771.68
279760-7976094.638100.50
378174-7817492.75698.53
479181-7918193.95199.87
579902-7990294.807100.79
682263-8226397.608103.61
极限180461-8046195.47094.692.17102.39101.562.12
280011-8001194.936101.75
376768-7676891.08897.79
479399-7939994.210101.06
580160-8016095.113102.05
682033-8203397.335104.31
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.608653186531862998652986482864740.12
214.678650086354864270.12
单位质量响应值RSD%判断
5922.885891.410.38数据可信
供试品溶液-2024102021批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min180441-8044195.54699.552.4895.5599.552.48
282728-8272898.26298.26
384198-84198100.008100.01
483704-8370499.42199.42
585611-85611101.687101.69
686171-86171102.352102.35
10min183691-8369199.406100.582.09100.36101.572.09
282524-8252498.02099.00
384286-84286100.113101.11
483910-8391099.666100.66
586964-86964103.294104.31
686677-86677102.953103.98
15min181761-8176197.11499.111.4499.06101.111.44
283429-8342999.095101.06
382423-8242397.90099.90
484436-84436100.291102.28
583632-8363299.336101.39
684951-84951100.903102.96
20min183093-8309398.69698.941.69101.62101.941.68
282678-8267898.203101.16
381818-8181897.181100.16
482681-8268198.206101.20
583633-8363399.337102.38
685905-85905102.036105.10
30min180942-8094296.14196.731.21100.05100.711.21
279843-7984394.83598.77
381203-8120396.451100.40
482484-8248497.972101.95
581956-8195697.345101.38
682210-8221097.647101.73
45min181264-8126496.52397.131.21101.39102.081.22
280873-8087396.059100.94
381297-8129796.562101.48
481798-8179897.158102.11
581747-8174797.097102.11
683663-8366399.373104.43
60min180629-8062995.76996.851.29101.60102.771.28
281179-8117996.422102.27
381376-8137696.656102.54
480688-8068895.839101.77
581916-8191697.298103.28
683435-8343599.102105.15
极限180454-8045495.56195.691.29102.35102.581.27
278867-7886793.676100.49
380405-8040595.503102.35
480479-8047995.591102.48
582027-8202797.430104.38
681141-8114196.377103.42
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