苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.608768387198872358705987228872810.28
214.678723487392873130.13
单位质量响应值RSD%判断
5978.155951.810.32数据可信
供试品溶液-2024101922批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min181344-8134495.68196.653.5395.6896.653.53
280185-8018594.31894.32
384847-8484799.80299.80
483878-8387898.66298.66
584984-8498499.96399.96
677765-7776591.47191.47
10min184162-8416298.996101.952.1099.95102.922.11
287016-87016102.353103.30
388788-88788104.437105.44
486952-86952102.278103.26
588228-88228103.779104.78
684910-8491099.876100.79
15min184487-8448799.378101.701.75101.33103.681.76
285319-85319100.357102.32
387875-87875103.363105.41
487583-87583103.020105.03
587917-87917103.413105.45
685563-85563100.644102.56
20min184619-8461999.534100.362.57102.47103.362.56
283834-8383498.610101.58
387875-87875103.363106.44
486715-86715101.999105.04
586803-86803102.102105.17
682065-8206596.52999.45
30min181649-8164996.04099.672.6499.98103.682.62
284216-8421699.060103.02
387982-87982103.489107.60
485933-85933101.079105.14
585521-85521100.595104.69
683119-8311997.769101.65
45min179934-7993494.02397.122.5498.92102.122.50
280781-8078195.01999.97
382945-8294597.564102.71
484729-8472999.663104.73
585113-85113100.115105.21
681882-8188296.314101.18
60min180295-8029594.44796.702.20100.28102.682.21
280992-8099295.267101.16
384383-8438399.256105.38
483703-8370398.456104.52
583378-8337898.074104.17
680524-8052494.717100.54
极限180260-8026094.40695.813.87101.19102.753.74
280563-8056394.763101.61
384234-8423499.081106.19
484009-8400998.816105.87
583546-8354698.271105.35
676106-7610689.52096.29
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.608678486895866938688986956868430.13
214.678692586931869280.01
单位质量响应值RSD%判断
5948.155925.560.27数据可信
供试品溶液-2024101923批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min182092-8209297.01897.502.8397.0297.502.83
279695-7969594.18694.19
381030-8103095.76395.76
485311-85311100.823100.82
585345-85345100.863100.86
681523-8152396.34696.35
10min183252-8325298.38999.791.9899.36100.771.98
282701-8270197.73898.68
382836-8283697.89898.86
485766-85766101.360102.37
585883-85883101.499102.51
686199-86199101.872102.84
15min182563-8256397.575100.121.9699.53102.091.96
284136-8413699.434101.35
383251-8325198.388100.32
485551-85551101.106103.13
585986-85986101.620103.64
686799-86799102.581104.56
20min181983-8198396.89098.561.7199.82101.531.71
281696-8169696.55099.46
382863-8286397.930100.85
485174-85174100.661103.69
584328-8432899.661102.70
684331-8433199.665102.67
30min180705-8070595.37997.132.1999.28101.092.18
279609-7960994.08497.96
381890-8189096.780100.68
483970-8397099.238103.28
584072-8407299.358103.39
682888-8288897.959101.96
45min178637-7863792.93596.843.6197.79101.773.51
279428-7942893.87098.69
380855-8085595.557100.42
483602-8360298.803103.83
582469-8246997.464102.49
686654-86654102.410107.39
60min179253-7925393.66395.022.0299.45100.922.01
278710-7871093.02198.78
379455-7945593.90299.73
483090-8309098.198104.22
581311-8131196.095102.10
680585-8058595.237101.25
极限179731-7973194.22894.491.39100.95101.341.43
278461-7846192.72799.42
378945-7894593.299100.06
481049-8104995.786102.79
581194-8119495.957102.92
680319-8031994.923101.88
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.608720187360871228698386876871080.22
214.678721987626874220.33
单位质量响应值RSD%判断
5966.305959.240.09数据可信
供试品溶液-2024102021批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min184556-8455699.49699.852.1399.5099.852.13
284973-8497399.98799.99
385668-85668100.804100.80
481542-8154295.94995.95
585549-85549100.664100.66
686853-86853102.199102.20
10min187584-87584103.059102.130.56104.05103.130.56
286432-86432101.703102.70
386987-86987102.356103.36
486215-86215101.448102.41
586702-86702102.021103.03
686856-86856102.202103.22
15min187931-87931103.467101.252.35105.49103.272.33
285201-85201100.255102.27
388025-88025103.578105.61
482617-8261797.21499.19
585811-85811100.973103.00
686683-86683101.999104.04
20min183610-8361098.38399.361.81101.44102.391.79
284633-8463399.586102.61
386479-86479101.759104.83
482593-8259397.186100.13
583396-8339698.131101.17
685916-85916101.096104.16
30min182657-8265797.26198.131.36101.31102.161.36
283443-8344398.186102.20
385104-85104100.141104.23
481947-8194796.426100.34
583001-8300197.666101.68
684213-8421399.092103.17
45min182234-8223496.76496.443.37101.78101.443.24
277334-7733490.99895.99
385561-85561100.678105.76
481388-8138895.768100.65
581510-8151095.912100.91
683723-8372398.516103.58
60min183099-8309997.78196.962.65103.77102.932.58
281499-8149995.899101.81
384465-8446599.389105.48
479121-7912193.10198.94
581302-8130295.667101.62
684894-8489499.894105.94
极限182342-8234296.89195.571.30103.85102.511.18
281304-8130495.669102.54
379397-7939793.425100.51
480833-8083395.115101.89
582120-8212096.629103.54
681334-8133495.705102.75
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