苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.608990490191900288982389968899830.16
214.678988290217900500.27
单位质量响应值RSD%判断
6163.226138.380.29数据可信
供试品溶液-2024101922批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min167682-6768277.20681.414.6877.2181.414.68
269609-6960979.40479.40
370115-7011579.98279.98
470021-7002179.87479.87
576682-7668287.47387.47
674096-7409684.52384.52
10min178148-7814889.14594.433.7189.9295.253.71
282501-8250194.11094.90
380312-8031291.61392.41
484559-8455996.45897.26
585136-8513697.11697.99
686055-8605598.16599.01
15min178359-7835989.38694.683.0791.0596.443.08
284301-8430196.16497.90
382516-8251694.12895.84
482616-8261694.24296.00
585149-8514997.13198.98
685042-8504297.00998.84
20min177585-7758588.50394.553.7691.0697.253.73
285645-8564597.697100.39
381158-8115892.57895.24
482797-8279794.44897.15
584804-8480496.73899.55
685319-8531997.325100.12
30min177523-7752388.43292.652.4491.8796.302.47
282332-8233293.91897.59
380408-8040891.72395.31
482088-8208893.63997.29
582446-8244694.04897.83
682546-8254694.16297.93
45min178508-7850889.55691.991.6993.8896.571.76
281614-8161493.09997.71
379848-7984891.08495.58
480230-8023091.52096.11
581609-8160993.09397.82
682061-8206193.60998.32
60min176040-7604086.74091.323.0991.9696.823.06
282680-8268094.31599.86
378209-7820989.21494.63
481202-8120292.62998.13
580556-8055691.89297.55
681650-8165093.14098.79
极限181803-8180393.31491.421.8299.4097.831.69
281293-8129392.73299.22
377925-7792588.89195.19
478973-7897390.08696.51
580396-8039691.70998.28
680476-8047691.80098.38
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.609007090126900569008390100900870.04
214.678994789985899660.03
单位质量响应值RSD%判断
6170.346132.650.44数据可信
供试品溶液-2024101923批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min171111-7111181.10984.022.9481.1184.022.94
273725-7372584.09084.09
371202-7120281.21381.21
474020-7402084.42784.43
575706-7570686.35086.35
676213-7621386.92886.93
10min179667-7966790.86893.393.4791.6894.233.45
277275-7727588.14088.98
384407-8440796.27497.09
482820-8282094.46495.31
584368-8436896.23097.09
682709-8270994.33795.21
15min180321-8032191.61495.242.5293.3397.012.51
282368-8236893.94995.67
385703-8570397.75299.53
482848-8284894.49696.28
583962-8396295.76797.59
685786-8578697.84799.66
20min179190-7919090.32494.142.6492.9696.862.61
282539-8253994.14496.81
384719-8471996.63099.38
481050-8105092.44595.18
582845-8284594.49397.28
684846-8484696.77599.57
30min178408-7840889.43293.492.7392.9797.162.70
281711-8171193.19996.80
383813-8381395.59799.32
481296-8129692.72696.38
581742-8174293.23596.96
684842-8484296.770100.53
45min179109-7910990.23194.052.8794.6698.652.82
280551-8055191.87696.41
383767-8376795.544100.22
485526-8552697.551102.14
582000-8200093.52998.19
683795-8379595.576100.30
60min177921-7792188.87692.542.6894.2198.082.65
279967-7996791.21096.66
381948-8194893.47099.10
482350-8235093.92899.49
580436-8043691.74597.34
684166-8416695.999101.68
极限178495-7849589.53190.663.1695.7697.133.05
276632-7663287.40693.77
382918-8291894.576101.14
480327-8032791.62198.12
577062-7706287.89794.41
681488-8148892.94599.59
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.608901089101887268888488835889110.17
214.678997690056900160.07
单位质量响应值RSD%判断
6089.796136.060.54数据可信
供试品溶液-2024102021批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min174580-7458085.60387.413.8785.6087.423.87
273607-7360784.48684.49
379352-7935291.08091.08
475150-7515086.25786.26
573877-7387784.79684.80
680377-8037792.25792.26
10min183850-8385096.24394.552.7497.1095.422.72
278338-7833889.91690.76
382897-8289795.14996.06
481472-8147293.51394.38
584680-8468097.19698.04
683021-8302195.29196.21
15min186101-8610198.82795.282.50100.6497.102.48
279650-7965091.42293.17
383298-8329895.60997.47
482404-8240494.58396.38
583399-8339995.72597.55
683215-8321595.51497.39
20min183386-8338695.71095.431.8298.5298.201.82
281309-8130993.32695.98
385121-8512197.702100.52
481647-8164793.71496.46
584478-8447896.96499.74
682886-8288695.13697.97
30min183419-8341995.74895.151.5599.5198.881.52
282883-8288395.13398.72
384731-8473197.254101.05
481375-8137593.40297.08
583470-8347095.80799.55
681517-8151793.56597.35
45min183564-8356495.91594.641.49100.6499.321.43
283673-8367396.040100.58
383358-8335895.678100.45
480794-8079492.73597.35
581816-8181693.90898.61
681534-8153493.58598.30
60min183001-8300195.26892.731.68100.9598.361.63
279897-7989791.70697.21
381820-8182093.91399.64
480623-8062392.53998.08
579784-7978491.57697.22
679615-7961591.38297.04
极限180848-8084892.79791.912.1199.4398.462.02
279250-7925090.96397.38
382725-8272594.952101.62
480531-8053192.43398.90
579264-7926490.97997.54
677828-7782889.33195.90
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