苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.609061790356905139045690272904430.15
214.679093091038909840.09
单位质量响应值RSD%判断
6194.736202.040.09数据可信
供试品溶液-2024101922批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min175848-7584885.85781.254.6585.8681.254.66
268279-6827977.28977.29
371004-7100480.37380.37
472741-7274182.34082.34
574937-7493784.82584.83
667858-6785876.81276.81
10min182748-8274893.66791.641.5394.5392.451.54
279238-7923889.69490.47
381477-8147792.22893.03
479951-7995190.50191.32
581328-8132892.06092.91
680994-8099491.68292.45
15min184071-8407195.16592.302.3096.9694.032.29
281265-8126591.98893.66
382420-8242093.29695.02
478739-7873989.12990.86
582446-8244693.32595.09
680286-8028690.88092.57
20min183173-8317394.14892.041.5896.9094.691.57
280393-8039391.00193.59
381917-8191792.72795.39
480029-8002990.58993.21
580207-8020790.79193.49
682123-8212392.96095.55
30min182015-8201592.83791.981.2796.5395.551.26
279839-7983990.37493.87
381029-8102991.72195.31
480450-8045091.06694.59
581578-8157892.34395.95
682641-8264193.54697.07
45min181749-8174992.53692.761.4397.1597.251.37
280935-8093591.61596.02
381427-8142792.17296.68
481434-8143492.18096.62
581892-8189292.69897.23
684232-8423295.34799.81
60min183254-8325494.24093.071.5699.7898.491.53
281241-8124191.96197.28
383381-8338194.38499.81
480471-8047191.09096.45
581585-8158592.35197.81
683389-8338994.39399.81
极限183940-8394095.01693.271.98101.5099.621.93
280855-8085591.52497.76
382820-8282093.749100.12
479907-7990790.45196.72
583492-8349294.509100.89
683363-8336394.363100.72
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.609090790892904619138390998909280.37
214.679108291209911460.10
单位质量响应值RSD%判断
6227.956213.090.17数据可信
供试品溶液-2024101923批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min170824-7082479.88579.601.3979.8879.601.39
270664-7066479.70479.70
368664-6866477.44877.45
471483-7148380.62880.63
571041-7104180.12980.13
670760-7076079.81279.81
10min184954-8495495.82288.944.8096.6289.734.75
275650-7565085.32886.13
381412-8141291.82792.60
478851-7885188.93889.74
577223-7722387.10287.90
675012-7501284.60885.41
15min182450-8245092.99890.282.8494.7591.962.82
278792-7879288.87290.52
383144-8314493.78195.47
479672-7967289.86591.56
578769-7876988.84690.52
677390-7739087.29188.93
20min183766-8376694.48290.133.4797.1792.723.44
280250-8025090.51693.06
381798-8179892.26294.89
480016-8001690.25392.85
577278-7727887.16489.73
676313-7631386.07688.59
30min179435-7943589.59788.902.2693.2392.392.25
278213-7821388.21991.66
381971-8197192.45896.01
478854-7885488.94292.44
577181-7718187.05590.49
677253-7725387.13690.51
45min181885-8188592.36190.182.2096.8994.562.17
278995-7899589.10193.43
381869-8186992.34396.82
478607-7860788.66393.05
577746-7774687.69292.00
680602-8060290.91395.16
60min179880-7988090.09989.531.1395.5594.821.15
279462-7946289.62894.85
380741-8074191.07096.47
478254-7825488.26593.54
579343-7934389.49394.67
678596-7859688.65193.81
极限180164-8016490.41989.961.1996.7796.141.06
279874-7987490.09296.21
378546-7854688.59494.91
478688-7868888.75594.91
580893-8089391.24297.32
680364-8036490.64596.69
苯磺酸左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.609109991101911169118890845910700.15
214.679203192084920580.05
单位质量响应值RSD%判断
6237.676275.260.43数据可信
供试品溶液-2024102021批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min171444-7144480.12280.723.1480.1280.723.14
269333-6933377.75477.75
371394-7139480.06580.07
471004-7100479.62879.63
576036-7603685.27185.27
672653-7265381.47781.48
10min182129-8212992.10489.192.4492.9189.992.42
277869-7786987.32788.10
381326-8132691.20492.00
477384-7738486.78387.58
580001-8000189.71890.57
678453-7845387.98288.80
15min183968-8396894.16790.343.8695.8992.043.81
274821-7482183.90985.56
382147-8214792.12493.84
480521-8052190.30191.97
580331-8033190.08891.84
681567-8156791.47493.17
20min180311-8031190.06590.852.3992.7393.452.35
278013-7801387.48889.98
381283-8128391.15693.79
482400-8240092.40894.98
580417-8041790.18492.84
683624-8362493.78196.39
30min178189-7818987.68691.462.9791.2594.972.88
278872-7887288.45291.82
383539-8353993.68697.23
483817-8381793.99797.49
582376-8237692.38195.93
682507-8250792.52896.08
45min181386-8138691.27191.281.5495.7195.711.55
279250-7925088.87693.12
382787-8278792.84297.32
482355-8235592.35896.79
581733-8173391.66096.14
680873-8087390.69695.17
60min180360-8036090.12091.001.2495.4796.341.22
280242-8024289.98895.13
382178-8217892.15997.57
481363-8136391.24596.60
580276-8027690.02695.42
682443-8244392.45697.84
极限180051-8005189.77491.911.3296.0398.161.21
282860-8286092.92498.96
382623-8262392.65898.99
482079-8207992.04898.32
582719-8271992.76699.06
681390-8139091.27697.58
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